Process for producing acesulfame potassium
AssigneeNutrinova Nutrition Specialists & Food Ingredients GmbH
InventorsMichael J. Bayer, Stephan Brietzke, Peter Groer, Christoph Mollenkopf
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AssigneeNutrinova Nutrition Specialists & Food Ingredients GmbH
InventorsMichael J. Bayer, Stephan Brietzke, Peter Groer, Christoph Mollenkopf
Estimating the term…
In one embodiment, the invention relates to processes for producing acesulfame potassium. In one embodiment, the process comprises the step of reacting a first reaction mixture to form an amidosulfamic acid salt such as a trialkyl ammonium amidosulfamic acid salt. The first reaction mixture comprises sulfamic acid, an amine, and smaller amounts, if any, acetic acid, e.g., less than 1 wt % (10000 wppm). In terms of ranges, the first reaction mixture may comprise from 1 wppm to 1 wt % acetic acid. The process further comprises the step of reacting the amidosulfamic acid salt with diketene to form an acetoacetamide salt. In preferred embodiments, the amidosulfamic acid salt formation reaction is conducted at pH levels from 5.5 to 7.0. The process further comprises the step of deriving the acesulfame-K from the acetoacetamide salt.
A process for producing acesulfame potassium, the process comprising the steps of:
A process for producing acesulfame potassium, the process comprising the steps of:
A process for producing acesulfame potassium, the process comprising the steps of:
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