Continuous transesterification method
AssigneeClariant Finance (BVI) Limited
InventorsMatthias Krull, Roman Morschhaeuser
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AssigneeClariant Finance (BVI) Limited
InventorsMatthias Krull, Roman Morschhaeuser
Estimating the term…
The invention relates to a continuous method for producing esters, in which at least one polyol ester of formula (I) (R1—COO)mR2 (I), where R1 represents hydrogen or an optionally substituted hydrocarbon group containing 1 to 50 carbon atoms, R2 represents an optionally substituted hydrocarbon group containing 2 to 10 carbon atoms, and m represents a number from 2 to 10 and is smaller than or equal to the number of carbon atoms in R2, is reacted with at least one monohydric alcohol of formula (II) R3—OH (II), where R3 represents an optionally substituted hydrocarbon group containing 1 to 30 C atoms, using microwave radiation in a reaction tube, the longitudinal axis of which extends in the direction of propagation of the microwaves of a single-mode microwave applicator, so as to obtain at least one ester of formula (III) R1—COO—R3 (III), where R1 and R3 have the meanings indicated above.
A continuous process for preparing esters, comprising the steps of providing a substantially microwave-transparent reaction tube, wherein the substantially microwave-transparent reaction tube has a longitudinal axis and wherein the longitudinal axis is parallel in direction to propagation of microwaves from a monomode microwave applicator,
Dependencies are inferred from the claim text.