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US 8,992,737 B2Granted
Trihalosilane refining method
AssigneeLG Chem, Ltd.
InventorsSung Kyu Lee, Joon Ho Shin, Jong Ku Lee, Sung Kyun Kim
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Abstract
A trihalosilane refining device and a trihalosilane refining method are provided. The trihalosilane refining device can be useful in obtaining high-purity trihalosilane from a feed containing a trihalosilane while consuming a small amount of energy.
Claims7
A trihalosilane refining method, comprising:
- introducing a feed containing a trihalosilane through an inlet port of a divided wall distillation column, which has an upper column region, a preliminary separation region, a main separation region and a lower column region formed therein and comprises the inlet port installed to introduce the feed containing the trihalosilane into the preliminary separation region, a first outlet port, a second outlet port and a third outlet port;
- and
- introducing an effluent, which flows out through the second outlet port formed at the 1/9 to 8/9 section of the divided wall section of the main separation region, into a first distillation column,
- wherein the second outlet port or the effluent flowing out through the second outlet port is maintained at a temperature of 86.4° C. to 116.4° C., and
- wherein the first distillation column is maintained at an operating pressure of −0.6 Kg/sqcmG to 9.0 Kg/sqcmG and an operating temperature of 37° C. to 145° C.
2 more elements
Dependencies are inferred from the claim text.