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US 8,986,734 B2Granted
Material with bacteriostatic properties
AssigneesCentre National De La Recherche Scientifique, Universite D'Orleans
InventorsRoland Benoit, Marie-Louise Saboungi, Fabienne Brulé
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Abstract
The invention relates to a method for making a composite material including a porous polymer matrix containing HEMA monomers and in which silver nanoparticles are dispersed, and to the use thereof as an anti-microbial material.
Claims8
A method for producing a composite material comprising a porous polymer matrix in which silver nanoparticles are dispersed, this method comprising the following steps:
- (a) mixing two compositions in a solvent selected from the group consisting of water and at least one alcohol to form a mixture, wherein the compositions comprise:
- (i) a first composition comprising a polymerizable fluid comprising HEMA monomer, wherein the HEMA monomer is present in the polymerizable fluid composition in monomer form, and
- (ii) a second composition comprising silver salts,
- wherein the mixture comprises:
- 58% to 63% by volume of HEMA monomer,
- 5% to 10% by volume of methanol,
- 1% to 5% by volume of isopropanol,
- 15% to 25% by volume of water, and
- 10−1 to 10−5 percent by mass of silver salts;
- and
- (b) irradiating the mixture of step (a) with gamma radiation with a dose flow rate greater than or equal to 2 kGray/hour, that causes the simultaneous polymerization of the HEMA monomer and the formation of silver nanoparticles, thereby producing the composite material comprising a porous polymer matrix in which silver nanoparticles are dispersed.
8 more elements
Dependencies are inferred from the claim text.