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US 8,974,642 B2Granted
Trihalosilane refining method
AssigneeLG Chem, Ltd.
InventorsSung Kyu Lee, Joon Ho Shin, Jong Ku Lee, Sung Kyun Kim
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Abstract
A trihalosilane refining device and a trihalosilane refining method are provided. The trihalosilane refining device can be useful in obtaining high-purity trihalosilane from a feed containing a trihalosilane while consuming a small amount of energy.
Claims7
A trihalosilane refining method, comprising:
- introducing a feed containing a trihalosilane into a divided wall distillation column having a divided wall, which has a length of at least 30% with respect to a total theoretical plate number thereof, installed therein;
- and
- introducing an effluent flowing out from the divided wall distillation column into a first distillation column,
- wherein the divided wall distillation column comprises an upper column region, a preliminary separation region, a main separation region and a lower column region, and has an inlet port installed therein to introduce the feed containing a trihalosilane into the preliminary separation region, a first outlet port, a second outlet port and a third outlet port,
- wherein the effluent flowing out through the second outlet port is introduced into the first distillation column,
- wherein the second outlet port or the effluent flowing out through the second outlet port is maintained at a temperature of 86.4° C. to 116.4° C., and
- wherein the first distillation column is maintained at an operating pressure of −0.6 Kg/sqcmG to 9.0 Kg/sqcmG and an operating temperature of 37° C. to 145° C.
4 more elements
Dependencies are inferred from the claim text.