Method for producing high-purity 1,5-pentanediol
AssigneeUbe Industries, Ltd.
InventorsYasutaka Yoshida, Kenji Hirotsu, Ryo Fujimoto, Ryousuke Katsura, Satoru Fujitsu, Takashi Doi, Kouichi Kashiwagi
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AssigneeUbe Industries, Ltd.
InventorsYasutaka Yoshida, Kenji Hirotsu, Ryo Fujimoto, Ryousuke Katsura, Satoru Fujitsu, Takashi Doi, Kouichi Kashiwagi
Estimating the term…
The present invention has an object to provide a method for efficiently producing high-purity 1,5-pentanediol by reacting tetrahydrofurfuryl alcohol with hydrogen. This manufacturing method for producing high-purity 1,5-pentanediol comprises: step (I): a step of obtaining a crude reaction product by a hydrogenolysis reaction of tetrahydrofurfuryl alcohol with hydrogen carried out in the presence of a copper-containing catalyst with reaction temperature of 200 to 350° C. and reaction pressure of 1 to 40 MPa until conversion rate of tetrahydrofurfuryl alcohol reaches 80% or less; step (II): a step of separating tetrahydrofurfuryl alcohol and crude 1,5-pentanediol (A) from the crude reaction product obtained in the step (I), and then, supplying recovered tetrahydrofurfuryl alcohol as a raw material for the step (I); and step (III): a step of obtaining the high-purity 1,5-pentanediol by distillation of the crude 1,5-pentanediol (A) obtained in the step (II).
A method for producing high-purity 1,5-pentanediol, the method comprising:
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