US 8,803,087 B2Granted

Spectrum analyzer and method of spectrum analysis

AssigneeKobe Steel, Ltd.

InventorsHirofumi Fukuyama, Shoichi Mure

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Abstract

A spectrum analysis method is provided in which a composition distribution of a sample in the depth direction is analyzed based on an energy spectrum of scattered particles scattered at the sample by irradiation with ion beams, the sample being composed of a single layer or multiple layers. In the spectrum analysis, the thickness of an object layer of the sample is obtained by the steps of measuring an energy spectrum of scattered particles scattered in a scattering angle (specific scattering angle) direction at which an energy spectrum corresponding to the object layer independently appears, extracting an independent energy spectrum of the object layer which independently appears in the measured energy spectrum, and calculating the thickness of the object layer based on a spectrum area surrounded by the waveform of the independent energy spectrum thus extracted. Since the thickness of the object layer is analyzed based on the spectrum area instead of using the half value width of the spectrum, the analysis processing can be rapidly performed and the accuracy of the analysis can be improved.

Claims7

Dependent claims

A spectrum analyzer analyzing a composition distribution of a sample in the depth direction based on an energy spectrum of scattered particles scattered at the sample by irradiation with ion beams, the sample including at least one object layer to be analyzed which contains at least one element, said spectrum analyzer comprising:

an ion beam generator;
scattering angle-setting means for setting a scattering angle of ion beams which are emitted from said ion beam generator and which are scattered at the sample, including a simulator for obtaining specific scattering angles where an independent energy spectrum of said at least one element of the object layer independently appears, and setting the scattering angle according to the specific scattering angles;
measured spectrum-obtaining means for obtaining a measured energy spectrum by measuring energy of scattered particles scattered in the direction of the scattering angle set by said scattering angle-setting means, the scattered particles being scattered from the sample when the sample is irradiated with the ion beams;
independent spectrum-extraction means for extracting an independent energy spectrum of said at least one element of the object layer which independently appears in the measured energy spectrum obtained by said measured spectrum-obtaining means;
means for obtaining a standard energy spectrum of a standard sample having a known composition distribution and layer thickness in the depth direction;
and
layer thickness-calculation means for calculating the thickness of the object layer based on a spectrum area surrounded by the waveform of the independent energy spectrum extracted by said independent spectrum-extraction means, wherein said layer thickness-calculation means calculates the thickness of the object layer by comparing the spectrum area surrounded by the waveform of the independent energy spectrum with a spectrum area surrounded by the waveform of the standard energy spectrum.

4 more elements

A spectrum analysis method for analyzing a composition distribution of a sample in the depth direction based on an energy spectrum of scattered particles scattered at the sample by irradiation with ion beams, the sample including at least one object layer to be analyzed, the spectrum analysis method comprising:

a step of obtaining specific scattering angles where an independent energy spectrum of said at least one element of the object layer independently appears;
a measured spectrum-obtaining step of obtaining a measured energy spectrum by measuring energy of scattered particles scattered in the direction of one of the specific scattering angles at which an energy spectrum corresponding to the object layer independently appears;
an independent spectrum-extraction step of extracting an independent energy spectrum of the object layer which independently appears in the measured energy spectrum obtained by the measured spectrum-obtaining step;
a step of obtaining a standard energy spectrum of a standard sample having a known composition distribution and layer thickness in the depth direction;
and
a layer thickness-calculation step of calculating the thickness of the object layer based on a spectrum area surrounded by the waveform of the independent energy spectrum extracted by the independent spectrum-extraction step, wherein said layer thickness-calculation step calculates the thickness of the object layer by comparing the spectrum area surrounded by the waveform of the independent energy spectrum with a spectrum area surrounded by the waveform of the standard energy spectrum,
wherein the specific scattering angle is searched by a process comprising:
a theoretical spectrum-obtaining step of obtaining theoretical energy spectra corresponding to predetermined scattering angles of the scattered particles by simulation based on a predefined distribution set beforehand for the sample in the depth direction;
and
a scattering angle-searching step of searching the scattering angle at which the energy spectrum corresponding to the object layer independently appears in the theoretical energy spectra obtained by the theoretical spectrum-obtaining step.

7 more elements

Dependencies are inferred from the claim text.