# US 8,784,995 B2 · Grain oriented electrical steel sheet and method for manufacturing the same

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- Number: US 8,784,995 B2
- Document ID: US8784995B2
- Status: Granted
- Kind: B2
- Application number: 13/821,608
- Filed: 2011-09-09
- Published: 2013-06-27
- Granted: 2014-07-22
- Earliest claimed: 2010-09-10
- Assignees: Jfe Steel Corporation
- Applicants: Takeshi Omura; Hirotaka Inoue; Hiroi Yamaguchi; Seiji Okabe; Yasuyuki Hayakawa
- Inventors: Takeshi Omura; Hirotaka Inoue; Hiroi Yamaguchi; Seiji Okabe; Yasuyuki Hayakawa
- Web page: https://patentgrep.com/patent/US8784995B2

## CPC

- C22C 38/00: Ferrous alloys, e.g. steel alloys (cast-iron alloys C22C37/00)
- C21D 8/12: during manufacturing of articles with special electromagnetic properties
- C21D 8/1233: {Cold rolling}
- C21D 8/1277: involving a particular surface treatment (C21D8/1294 takes precedence)
- C21D 8/1283: {Application of a separating or insulating coating}
- C22C 38/001: {containing N}
- C22C 38/02: containing silicon
- C22C 38/04: containing manganese
- C22C 38/06: containing aluminium
- C22C 38/08: containing nickel {(C22C38/105 takes precedence)}
- C22C 38/34: with more than 1.5% by weight of silicon
- C22C 38/60: containing lead, selenium, tellurium, or antimony, or more than 0.04% by weight of sulfur
- H01F 1/16: in the form of sheets (H01F1/147 takes precedence)
- C21D 2201/05: Grain orientation
- C22C: ALLOYS (treatment of alloys C21D, C22F)
- C21D: MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING (surface treatment of metallic material involving at least one process provided for in class C23 and at least one process covered by this subclass C23F17/00; unidirectional solidification of eutectic materials or unidirectional demixing of eutectoid materials C30B)
- H01F: MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES

## Abstract

A grain oriented electrical steel sheet has linear grooves for magnetic domain refinement formed on a surface thereof and may reduce iron loss by using these linear grooves, where the proportion of those linear grooves having crystal grains directly beneath themselves, each crystal grain having an orientation deviating from the Goss orientation by 10° or more and a grain size of 5 μm or more, is controlled to 20% or less, and secondary recrystallized grains are controlled to have an average β angle of 2.0° or less, and each secondary recrystallized grain having a grain size of 10 mm or more is controlled to have an average β-angle variation of 1° to 4°.

## Claims

### Claim 1

A grain oriented electrical steel sheet comprising: a forsterite film and tension coating on a surface of the steel sheet; and linear grooves for magnetic domain refinement on the surface of the steel sheet,
wherein a proportion of linear grooves, each having crystal grains directly beneath itself, each crystal grain having an orientation deviating from a Goss orientation by 10° or more and a grain size of 5 μm or more, is 20% or less, and
wherein secondary recrystallized grains are controlled to have an average β-angle of 2.0° or less, and each secondary recrystallized grain having a grain size of 10 mm or more has an average β-angle variation range of 1° to 4°.

### Claim 2 (depends on 1)

A method of manufacturing a grain oriented electrical steel sheet according to claim 1, comprising:
subjecting a slab for a grain oriented electrical steel sheet to hot rolling to obtain a hot-rolled steel sheet;
then, optionally, subjecting the steel sheet to hot band annealing;
subjecting the steel sheet to subsequent cold rolling once, or twice or more with intermediate annealing performed therebetween, to be finished to a final sheet thickness; subjecting the steel sheet to subsequent decarburization;
then applying an annealing separator mainly composed of MgO to a surface of the steel sheet before subjecting the steel sheet to final annealing; and
subjecting the steel sheet to subsequent tension coating,
wherein
(1) linear grooves are formed in a widthwise direction of the steel sheet by electrolytic etching before the final annealing to form a forsterite film,
(2) an average cooling rate at a temperature of at least 750° C. to 350° C. is 40° C./s or higher during cooling at the time of the hot band annealing,
(3) an average heating rate at a temperature of at least 500° C. to 700° C. is 50° C./s or higher during heating at the time of the decarburization, and
(4) the final annealing is performed on the steel sheet in the form of a coil having a diameter of 500 mm to 1500 mm.