# US 8,784,658 B2 · Wastewater treatment process and plant comprising controlling the dissolved oxygen concentration

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- Number: US 8,784,658 B2
- Document ID: US8784658B2
- Status: Granted
- Kind: B2
- Application number: 12/742,158
- Filed: 2008-11-14
- Published: 2010-11-04
- Granted: 2014-07-22
- Earliest claimed: 2007-11-16
- Assignees: Bluewater Bio Technologies Limited
- Applicants: Garry Hoyland
- Inventors: Garry Hoyland
- Web page: https://patentgrep.com/patent/US8784658B2

## CPC

- C02F 3/02: Aerobic processes
- C02F 3/104: {Granular carriers}
- C02F 3/12: Activated sludge processes
- C02F 3/301: {Aerobic and anaerobic treatment in the same reactor}
- C02F 3/341: {Consortia of bacteria}
- C02F 3/345: {for biological oxidation or reduction of sulfur compounds}
- C02F 3/302: {Nitrification and denitrification treatment (C02F3/308 takes precedence)}
- C02F 3/308: {Biological phosphorus removal}
- C02F 2103/22: from the processing of animals, e.g. poultry, fish, or parts thereof
- C02F 2209/001: Upstream control, i.e. monitoring for predictive control
- C02F 2209/22: O2
- Y02W 10/10: Biological treatment of water, waste water, or sewage
- C02F: TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE (separation in general B01D; special arrangements on waterborne vessels of installations for treating water, waste water or sewage, e.g. for producing fresh water, B63J; adding materials to water to prevent corrosion C23F; treating radioactively-contaminated liquids G21F9/04; regeneration of reactants for recirculation into processes, see the relevant places for the processes)
- Y02W: CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT

## Abstract

The present invention relates to a process for treating wastewater that includes the steps of: —a contact step, wherein wastewater contacts bacteria retained on a support surface and the dissolved oxygen concentration of the wastewater is maintained at 2.0 mg/l or less; an aeration step, wherein gas is passed through wastewater that has passed through the contact step and the dissolved oxygen concentration of the wastewater is reduced as the wastewater passes through the aeration step; a sedimentation step, wherein wastewater that has passed through the aeration step is substantially separated into treated water and sludge; and a sludge recycling step, wherein sludge from the sedimentation step is passed to the contact step. The invention also relates to a processing unit on which the aforementioned process may be operated.

## Claims

### Claim 1

A process for treating wastewater comprising:
a. a contact step, wherein wastewater contacts bacteria retained on a support surface and the dissolved oxygen concentration of the wastewater is maintained at 1.0 mg/l or less, wherein the wastewater is maintained at the dissolved oxygen concentration by control of the supply of the oxygen to the wastewater;
b. an aeration step, wherein gas is passed through wastewater that has passed through the contact step and the dissolved oxygen concentration of the wastewater is reduced as the wastewater passes through the aeration step;
c. a sedimentation step, wherein wastewater that has passed through the aeration step is substantially separated into treated water and sludge; and
d. a sludge recycling step, wherein sludge from the sedimentation step is continuously passed to the contact step.

### Claim 2 (depends on 1)

A process as claimed in claim 1, wherein the dissolved oxygen concentration of wastewater in the contact step is maintained at from 0.2 to 1.0 mg/l.

### Claim 3 (depends on 1)

A process as claimed in claim 1, wherein the dissolved oxygen concentration of wastewater in the contact step is maintained at a range of from 0.5 to 1.0 mg/l.

### Claim 4 (depends on 1)

A process as claimed in claim 1, wherein the dissolved oxygen concentration of wastewater towards the beginning of the wastewater's passage through the aeration step encourages growth and development of bacteria, and a reduced concentration of nutrients and the controlled dissolved oxygen concentration of wastewater towards the end of the wastewater's passage through the aeration step encourage sporulation of the bacteria.

### Claim 5 (depends on 1)

A process as claimed in claim 1, wherein the dissolved oxygen concentration of wastewater towards the beginning of the aeration step is in the range of from 0.5 to 1.0 mg/l.

### Claim 6 (depends on 1)

A process as claimed in claim 1, wherein the dissolved oxygen concentration of wastewater towards the end of the aeration step is in the range of from 0 to 0.3 mg/l.

### Claim 7 (depends on 1)

A process as claimed in claim 1, wherein the wastewater takes at least 4 hours to pass through the aeration step.

### Claim 8 (depends on 1)

A process as claimed in claim 1, wherein the dissolved oxygen concentration of the wastewater continuously reduces as it passes through the aeration step.

### Claim 9 (depends on 8)

A process as claimed in claim 8, wherein control of supply of oxygen comprises a monitoring step in which the dissolved oxygen concentration of the wastewater is measured and compared against the desired concentration, and a feedback step in which the means of delivering the oxygen to the wastewater is controlled in order to increase or decrease the supply of oxygen to the wastewater so as to arrive at the desired dissolved oxygen concentration of wastewater.

### Claim 10 (depends on 1)

A process as claimed in claim 1, wherein the supply of oxygen to the wastewater is varied in order to maintain the wastewater at the recited dissolved oxygen concentrations.

### Claim 11 (depends on 1)

A process as claimed in claim 1, wherein the bacteria is a spore forming Bacteria.

### Claim 12 (depends on 11)

A process as claimed in claim 11, wherein the bacteria is from at least one of Bacillus and Clostridium genera.

### Claim 13 (depends on 12)

A process as claimed in claim 12, wherein the bacteria is B. subtilis, B. vallismortis, B. amyloliquefaciens, B. licheniformis and B. megaterium, or any combination thereof.

### Claim 14 (depends on 1)

A process as claimed in claim 1, wherein the bacteria is a mutant or variant of at least one of Bacillus and Clostridium genera and is capable of forming spores and of breaking down molecules that comprise nitrogen, carbon, sulphur, chlorine and/or phosphorous.

### Claim 15 (depends on 1)

A process as claimed in claim 1, wherein the bacteria are mixed species populations.

### Claim 16 (depends on 1)

A process as claimed in claim 1, wherein the sludge forms a blanket in the sedimentation tank and the blanket depth is maintained at 1 m or above.

### Claim 17 (depends on 1)

A process as claimed in claim 1, wherein the sludge forms a blanket in the sedimentation tank and the sludge retained within the blanket clears from the sedimentation tank with a downward velocity of from 0.3-1.5 m/h.

### Claim 18 (depends on 1)

A process as claimed in claim 1, wherein the sludge is retained in the sedimentation tank for 1 hour or more.

### Claim 19 (depends on 1)

A process as claimed in claim 1, wherein the support surface is a reticulated structure with a void that makes up more than 95% of the reticulated surface's total volume.

### Claim 20 (depends on 1)

A process as claimed in claim 1, wherein the support surface comprises any one or more of the following synthetic polymers:-polypropylene, polyester, polyurethane, polyether-polyurethane, polyvinyl chloride, polyvinylidene chloride and polyvinylidene fluoride, or any combination thereof.

### Claim 21

A unit for treating wastewater, wherein the unit comprises:—
(a) a contact tank, which includes a support surface on which bacteria are retained and that is positioned so as to come into contact with wastewater retained in the contact tank;
(b) an aeration tank that includes means for passing gas through wastewater retained within the aeration tank;
(c) a conduit provided between the contact tank and aeration tank and through which wastewater can pass from the contact tank to the aeration tank;
(d) a sedimentation tank;
(e) a conduit provided between the aeration tank and the sedimentation tank and through which wastewater can pass from the aeration tank to the sedimentation tank;
(f) a conduit provided between the sedimentation tank and the contact tank and through which sediment can pass continuously from the sedimentation tank to the contact tank; and
(g) a wastewater dissolved oxygen concentration control means capable of maintaining the dissolved concentration of wastewater retained in the contact tank at 1.0 mg/l or less and capable of reducing the dissolved oxygen concentration of wastewater as it passes through the aeration tank or tanks.

### Claim 22 (depends on 14)

A process as claimed in claim 14, wherein the bacteria is a mutant or variant of Bacillus genera and is selected from the group consisting of B. subtilis, B. vallismortis, B. amyloliquefaciens, B. licheniformis and B. megaterium, or any combination thereof.
