# US 8,784,517 B1 · Polycrystalline diamond compacts, methods of fabricating same, and applications therefor

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- Number: US 8,784,517 B1
- Document ID: US8784517B1
- Status: Granted
- Kind: B1
- Application number: 12/717,158
- Filed: 2010-03-04
- Granted: 2014-07-22
- Earliest claimed: 2009-03-05
- Assignees: US Synthetic Corporation
- Applicants: Jair J. Gonzalez; David P. Miess; Mark P. Chapman; Steven L. Choate; D. Bart Crockett; Jeffery A. Gerber
- Inventors: Jair J. Gonzalez; David P. Miess; Mark P. Chapman; Steven L. Choate; D. Bart Crockett; Jeffery A. Gerber
- Web page: https://patentgrep.com/patent/US8784517B1

## CPC

- B24D 18/00: Manufacture of grinding tools {or other grinding devices}, e.g. wheels, not otherwise provided for
- B24D 3/00: Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents
- B24D 18/0009: {using moulds or presses}
- B24D 99/005: {Segments of abrasive wheels}
- C04B 35/52: based on carbon, e.g. graphite
- C04B 35/645: Pressure sintering
- C04B 37/026: {consisting of metals or metal salts}
- C04B 2235/427: Diamond
- C04B 2235/5436: micrometer sized, i.e. from 1 to 100 micron
- C04B 2235/5472: Bimodal, multi-modal or multi-fraction
- C04B 2235/80: Phases present in the sintered or melt-cast ceramic products other than the main phase
- C04B 2237/363: Carbon
- C04B 2237/401: Cermets
- C04B 2237/61: Joining two substrates of which at least one is porous by infiltrating the porous substrate with a liquid, such as a molten metal, causing bonding of the two substrates, e.g. joining two porous carbon substrates by infiltrating with molten silicon
- B24D: TOOLS FOR GRINDING, BUFFING OR SHARPENING (abrading-bodies specially designed for tumbling apparatus, e.g. abrading-balls B24B31/14; honing tools B24B33/08; lapping tools B24B37/11)
- C04B: LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE {(roofing granules E04D7/005)}; CERAMICS (devitrified glass-ceramics C03C10/00); REFRACTORIES; TREATMENT OF NATURAL STONE

## Abstract

Embodiments of the invention relate to polycrystalline diamond compacts (“PDCs”) including a pre-sintered polycrystalline diamond (“PCD”) table that may exhibit a non-cylindrical-shaped geometry and/or may have been partially graphitized prior to bonding to a substrate in a high-pressure/high-temperature process (“HPHT”). The disclosed PDCs may be used in a variety of applications, such as rotary drill bits, mining tools, drill bits, bearing apparatuses, wire-drawing dies, machining equipment, and other articles and apparatuses.

## Claims

### Claim 1

A method of fabricating a polycrystalline diamond compact, comprising:
providing an at least partially leached polycrystalline diamond table including a plurality of interstitial regions therein, wherein the at least partially leached polycrystalline diamond table exhibits a non-cylindrical-shaped geometry;
partially graphitizing the at least partially leached polycrystalline diamond table to form a partially graphitized polycrystalline diamond table;
positioning the partially graphitized polycrystalline diamond table adjacent to a substrate; and
subjecting the partially graphitized polycrystalline diamond table and the substrate to a high-pressure/high-temperature process to form the polycrystalline diamond compact.

### Claim 2 (depends on 1)

The method of claim 1 wherein subjecting the at least partially leached polycrystalline diamond table and the substrate to a high-pressure/high-temperature process to form the polycrystalline diamond compact comprises infiltrating the at least partially leached polycrystalline diamond table with a metallic infiltrant from the substrate.

### Claim 3 (depends on 2)

The method of claim 2, further comprising at least partially removing the metallic infiltrant from the infiltrated polycrystalline diamond table.

### Claim 4 (depends on 1)

The method of claim 1 wherein the substrate comprises a cemented carbide substrate.

### Claim 5 (depends on 1)

The method of claim 1 wherein partially graphitizing the at least partially polycrystalline diamond table to form a partially graphitized polycrystalline diamond table comprises heat-treating the at least partially leached polycrystalline diamond table under graphite stable conditions.

### Claim 6

A method of fabricating a polycrystalline diamond compact, comprising:
providing an at least partially leached polycrystalline diamond table including a plurality of interstitial regions therein;
partially graphitizing the at least partially leached polycrystalline diamond table to form a partially graphitized polycrystalline diamond table;
positioning the partially graphitized polycrystalline diamond table adjacent to a substrate; and
infiltrating the partially graphitized polycrystalline diamond table with a metallic infiltrant.

### Claim 7 (depends on 6)

The method of claim 6 wherein the at least partially leached polycrystalline diamond table exhibits a non-cylindrical-shaped geometry.

### Claim 8 (depends on 6)

The method of claim 6 wherein the substrate comprises a cemented carbide substrate.

### Claim 9 (depends on 6)

The method of claim 6 wherein partially graphitizing the at least partially leached polycrystalline diamond table to form a partially graphitized polycrystalline diamond table comprises heat-treating the at least partially leached polycrystalline diamond table under graphite stable conditions.

### Claim 10 (depends on 6)

The method of claim 6 wherein partially graphitizing the at least partially leached polycrystalline diamond table to form a partially graphitized polycrystalline diamond table comprises partially graphitizing about 5 volume percent or less of the at least partially leached polycrystalline diamond table.

### Claim 11 (depends on 6)

The method of claim 6 wherein partially graphitizing the at least partially leached polycrystalline diamond table to form a partially graphitized polycrystalline diamond table comprises partially graphitizing about 2 to about 4 volume percent of the at least partially leached polycrystalline diamond table.

### Claim 12 (depends on 6)

The method of claim 6 wherein partially graphitizing the at least partially leached polycrystalline diamond table to form a partially graphitized polycrystalline diamond table comprises partially graphitizing about 0.5 to about 1.5 volume percent of the at least partially leached polycrystalline diamond table.

### Claim 13 (depends on 6)

The method of claim 6 wherein the substrate comprises the metallic infiltrant.
