# US 8,783,091 B2 · Cement testing

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- Number: US 8,783,091 B2
- Document ID: US8783091B2
- Status: Granted
- Kind: B2
- Application number: 12/607,560
- Filed: 2009-10-28
- Published: 2011-04-28
- Granted: 2014-07-22
- Earliest claimed: 2009-10-28
- Assignees: Halliburton Energy Services, Inc.
- Applicants: David L. Meadows; Robert P. Darbe; Keith D. Pewitt
- Inventors: David L. Meadows; Robert P. Darbe; Keith D. Pewitt
- Web page: https://patentgrep.com/patent/US8783091B2

## CPC

- G01N 3/08: by applying steady tensile or compressive forces (G01N3/28 takes precedence)
- G01N 3/12: Pressure testing
- G01N 33/383: {Concrete or cement}
- G01N 2203/0019: Compressive
- G01N 2203/0048: Hydraulic means
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)

## Abstract

Devices and methods for testing cement include: a pressure vessel with a sample container inside an interior working volume of the pressure vessel, the pressure vessel configured to supply a first pressurized fluid to control a pore pressure of a cement sample and to supply a second pressurized fluid to lateral exterior surfaces of the sample container to provide a confining pressure that can be different than the pore pressure.

## Claims

### Claim 1

A system for testing cement, the system comprising:
at least one cement testing apparatus, each cement testing apparatus comprising:
a pressure vessel defining: a working volume inside the pressure vessel, the pressure vessel defining a first channel providing liquid communication through the pressure vessel to the working volume of the pressure vessel and a second channel providing liquid communication through the pressure vessel to the working volume of the pressure vessel; and
a substantially tubular sample container comprising walls extending from a first end with a first end member having an opening to a second end with a second end member having an opening, the end members configured to grip ends of a cement sample in the sample container, the sample container disposed in the working volume of the pressure vessel with the sample container substantially sealed to prevent liquid communication between a sample volume, defined by the first and second end members and a tubular member of the sample container, and portions of the working volume of the pressure vessel outside the sample container, the tubular member comprising a specified material that is more flexible than a material of the first and second end members, the tubular member comprising walls that are substantially sealed to the first end member and the second end member;
wherein the sample container is positioned such that the first channel provides liquid communication through the pressure vessel to the sample volume of the sample container; and the second channel provides liquid communication through the pressure vessel to the portions of the working volume of the pressure vessel outside the sample container.

### Claim 2 (depends on 1)

The system of claim 1, each of the end members of the sample container defining an internal cavity that has a first transverse cross-sectional dimension adjacent the tubular member and a second transverse cross-section spaced apart from tubular member that is larger than the first cross-sectional dimension.

### Claim 3 (depends on 1)

The system of claim 1, the first end member of the sample container having a face extending across a first open end of the sample container, the first end member defining a channel in liquid communication with a channel defined in a first end cap of the pressure vessel and extending to an opening in the face of the first end member.

### Claim 4 (depends on 3)

The system of claim 3, the second end member having a face extending across a second open end of the sample container, the second end member defining a frusto-conical cavity extending from an opening in the face of the second end member.

### Claim 5 (depends on 1)

The system of claim 1, the pressure vessel comprising:
a first end cap;
a second end cap; and
a sidewall member extending between the first end cap and the second end cap.

### Claim 6 (depends on 5)

The system of claim 5, the first end cap of the pressure vessel defining the first channel through the end cap to the working volume of the pressure vessel.

### Claim 7 (depends on 6)

The system of claim 6, the second end cap defining a third channel extending through the second end cap.

### Claim 8 (depends on 5)

The system of claim 5, further comprising a piston extending through an aperture in the second end cap of the pressure vessel.

### Claim 9 (depends on 8)

The system of claim 8, the piston defining a channel extending through the piston, the channel in the piston providing liquid communication between an exterior of the pressure vessel and the second end member of the sample container.

### Claim 10 (depends on 1)

The system of claim 1, the at least one cement testing apparatus comprising a plurality of the cement testing apparatuses.

### Claim 11 (depends on 10)

The system of claim 10, the system further comprising:
a first pressure source operable to selectively supply pressurized liquid to the first channels of the plurality of cement testing apparatuses; and
a second pressure source operable to selectively supply pressurized liquid to the second channels of the plurality of cement testing apparatuses.

### Claim 12 (depends on 1)

The system of claim 1, the material of the tubular member comprising a rubber material, and the material of the first and second end members comprising a steel material.

### Claim 13

A system for testing cement, the system comprising:
at least one cement testing apparatus, each cement testing apparatus comprising:
a pressure vessel defining: (i) a working volume inside the pressure vessel, (ii) a first channel providing liquid communication through the pressure vessel to the working volume of the pressure vessel, and (iii) a second channel providing liquid communication through the pressure vessel to the working volume of the pressure vessel; and
a substantially tubular sample container defining a sample volume inside the sample container, the sample container comprising:
a first end member;
a second end member, the first and second end members configured to grip ends of a cement sample in the sample container;
walls extending from a first end with an opening to a second end with an opening, the sample container disposed in the working volume of the pressure vessel with the sample container substantially sealed to prevent liquid communication between the sample volume of the sample container and portions of the working volume of the pressure vessel outside the sample container; and
a tubular member having walls that are substantially sealed to the first end member and the second end member, the tubular member comprising a material that is more flexible than a material of the first and second end members,
wherein the sample container is positioned such that the first channel provides liquid communication through the pressure vessel to the sample volume of the sample container; and the second channel provides liquid communication through the pressure vessel to the portions of the working volume of the pressure vessel outside the sample container.
