# US 8,772,045 B1 · Method for explosives detection > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 8,772,045 B1 - Document ID: US8772045B1 - Status: Granted - Kind: B1 - Application number: 13/068,937 - Filed: 2011-05-23 - Granted: 2014-07-08 - Earliest claimed: 2003-11-07 - Applicants: Jeffrey S. Haas - Inventors: Jeffrey S. Haas - Web page: https://patentgrep.com/patent/US8772045B1 ## CPC - G01N 33/22: Fuels; Explosives - G01N 33/227: {Explosives, e.g. combustive properties thereof} - G01N 31/22: using chemical indicators (G01N31/02 takes precedence) - Y10T 436/25: including sample preparation - G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q) - Y10T: TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION ## Abstract The present method and system may be used for detecting the presence of explosive elements. A sample element may be used to swipe an object for a test sample. The sample element may be positioned in a sample holder of a testing device having a heater. The heater may be programmed to heat the sample element and sample in a controlled manner through two temperature increases from approximately 35 degrees to 165 degrees centigrade in approximately 20 seconds. Prior to each temperature increase a first and second reagent fluid is applied to the sample holder, and during the temperature rise the sample holder is observed for the presence of various explosive elements by detecting colors as compared to a color chart. The color observations may be based on time and temperature variations using a testing device. ## Claims ### Claim 1 A method for detecting the presence of explosive elements comprising: a) swiping an object to obtain a test sample using a sample element having a swipe pad; b) placing said sample element in a sample holder in a testing device and retaining said sample element with a sample retainer; c) applying a first reagent fluid that is a solution of a tetrabutylammonium hydroxide, an ethanol and a water from a fluid container on said swipe pad; d) activating a heater disposed under said sample element; e) heating said swipe pad to a first temperature from approximately 35 degrees to approximately 135 degrees centigrade to activate said first reagent fluid with said test sample; f) viewing said swipe pad to observe any color change in said test sample; g) applying a second reagent fluid that is a solution of a phosphoric acid, a sulfanilic acid, N-(1-naphthyl)ethylenediamine dihydrochloride and a water from a second fluid container on said swipe pad; h) activating said heater; i) heating said swipe pad to a second temperature from approximately 135 degrees to approximately 165 degrees centigrade to activate said second reagent fluid with said test sample; and j) viewing said swipe pad to observe any described sequence of color change in said test sample over time and heat profile that may occur. ### Claim 2 (depends on 1) The method as in claim 1 wherein said first temperature heating is completed in approximately 8 to 10 seconds and said second temperature heating is completed in approximately 8 to 10 seconds. ### Claim 3 (depends on 1) The method as in claim 1 wherein said swipe pad has an approximately circular shape of approximately 0.67 inch diameter and an approximate thickness of 0.001 to 0.003 inches. ### Claim 4 (depends on 1) The method as in claim 1 wherein said swipe pad is formed of a woven approximately 100 percent continuous filament virgin polyester material. ### Claim 5 (depends on 1) The method as in claim 1 wherein approximately 20 to 50 microliters of said first reagent fluid and later after heating, 20 to 50 microliters of said second reagent fluid are applied to said swipe pad. ### Claim 6 (depends on 1) The method as in claim 1 wherein said tetrabutylammonium hydroxide in said water solution is in the approximate range of 0.1 to 1.53 Molar, and said ethanol is between approximate 5 and 95 percent of said water solution. ### Claim 7 (depends on 1) The method as in claim 1 wherein said tetrabutylammonium hydroxide in said water solution is in the approximate range of 0.7 to 0.9 Molar, and said ethanol is approximately 35 percent of said water solution. ### Claim 8 (depends on 1) The method as in claim 1 wherein: said phosphoric acid is in a water solution in the approximate range of 1.0 to 4.0 Molar; and said sulfanilic acid is approximately 8 grams mixed with said N-(1-naphthyl)ethylenediamine dihydrochloride of approximately 5 grams per 1000 milliliters of said phosphoric acid in said water solution. ### Claim 9 (depends on 1) The method as in claim 1 wherein: said phosphoric acid is in a water solution in the approximate range of 0.1 to 7.35 Molar; and said sulfanilic acid is approximately 5 to 8 grams mixed with said N-(1-naphthyl)ethylenediamine dihydrochloride of approximately 5 to 9 grams per 1000 milliliters of said phosphoric acid in said water solution. ### Claim 10 A method for detecting the presence of explosive elements comprising: swiping an object to obtain a test sample using a sample element having a swipe pad that is an approximately circular shape of approximately 0.75 inch diameter and an approximate thickness of 0.002 to 0.005 inches; placing said sample element in a sample holder in a testing device and retaining said sample element with a sample retainer; applying a first reagent fluid of approximately 20 to 50 microliters from a fluid retainer on said swipe pad; activating a heater disposed under said sample element; heating said swipe pad to a temperature to activate said first reagent fluid with said test sample; viewing said swipe pad to observe any described sequence of color change in said test sample over time and heat profile; applying a second reagent fluid of approximately 20 to 50 microliters from a second fluid retainer on said swipe pad; and viewing said swipe pad to observe any described sequence of color change in said test sample over time and heat profile. ### Claim 11 (depends on 10) The method as in claim 10 wherein said temperature is approximately 150° C. ### Claim 12 (depends on 10) The method as in claim 10 wherein said swipe pad is formed of a woven approximately 100 percent continuous filament virgin polyester material.