# US 8,770,499 B2 · Method for manufacturing powder

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- Number: US 8,770,499 B2
- Document ID: US8770499B2
- Status: Granted
- Kind: B2
- Application number: 14/003,609
- Filed: 2012-02-24
- Published: 2013-12-19
- Granted: 2014-07-08
- Earliest claimed: 2011-03-16
- Assignees: Nisshin Seifun Group Inc.
- Applicants: Kazumi Kozawa; Kosuke Ando; Daisuke Sato
- Inventors: Kazumi Kozawa; Kosuke Ando; Daisuke Sato
- Web page: https://patentgrep.com/patent/US8770499B2

## CPC

- B02C 23/18: Adding fluid, other than for crushing or disintegrating by fluid energy ({for tumbling mills B02C17/186;} feeding devices B02C23/02)
- B02C 19/061: {of the cylindrical type (B02C19/068 takes precedence)}
- C04B 35/6261: {Milling}
- C04B 35/6263: {characterised by their solids loadings, i.e. the percentage of solids}
- C04B 35/6264: {Mixing media, e.g. organic solvents}
- C04B 35/62655: {Drying, e.g. freeze-drying, spray-drying, microwave or supercritical drying}
- C04B 2235/3236: Alkaline earth titanates
- C04B 2235/5445: submicron sized, i.e. from 0,1 to 1 micron
- C04B 2235/5481: Monomodal
- B02C: CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN ({household tools and machines for pulverising foodstuffs, e.g. coffee and spice mills A47J42/00; pharmaceutical mortars A61J3/02; mechanical processing of refuse and garbage B03B9/06; dressing mould materials by grinding B22C5/04}; obtaining metallic powder by crushing, grinding or milling B22F9/04; {recovery of plastics by disintegrating B29B17/00; crushing raw materials in starch making C08B30/02; beaters for papermaking D21D1/02; crushing devices specially for transport in mines E21F13/002; slag crushing devices F23J1/00; fuel milling devices in combustion apparatus F23K1/00; household devices for crushing coal F24B15/02; ice disintegrating devices F25C5/02})
- C04B: LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE {(roofing granules E04D7/005)}; CERAMICS (devitrified glass-ceramics C03C10/00); REFRACTORIES; TREATMENT OF NATURAL STONE

## Abstract

A method for manufacturing a powder includes a mixing step in which a powder and a liquid additive are mixed together, a drying step in which the powder mixed in the mixing step is dried, a loading step in which the powder dried in the drying step is loaded into a pulverizer, a heating step in which a high-pressure gas is heated, a supplying step in which the high-pressure gas heated in the heating step is supplied to the pulverizer, and a pulverizing step in which the powder is pulverized by the pulverizer.

## Claims

### Claim 1

A method for manufacturing a powder comprising:
a mixing step in which a powder and a liquid additive are mixed together;
a drying step in which the powder mixed in the mixing step is dried;
a loading step in which the powder dried in the drying step is loaded into a pulverizer;
a heating step in which a high-pressure gas is heated;
a supplying step in which the high-pressure gas heated in the heating step is supplied to the pulverizer; and
a pulverizing step in which the powder is pulverized by the pulverizer.

### Claim 2 (depends on 1)

The method for manufacturing a powder according to claim 1, wherein the liquid additive is diethylene glycol monomethyl ether.

### Claim 3 (depends on 2)

The method for manufacturing a powder according to claim 2, wherein the powder is a powder including barium titanate.

### Claim 4 (depends on 3)

The method for manufacturing a powder according to claim 3, wherein a drying temperature and a period of time for drying in the drying step correspond to a flash point of the liquid additive.

### Claim 5 (depends on 2)

The method for manufacturing a powder according to claim 2, wherein a drying temperature and a period of time for drying in the drying step correspond to a flash point of the liquid additive.

### Claim 6 (depends on 1)

The method for manufacturing a powder according to claim 1, wherein the powder is a powder including barium titanate.

### Claim 7 (depends on 6)

The method for manufacturing a powder according to claim 6, wherein a drying temperature and a period of time for drying in the drying step correspond to a flash point of the liquid additive.

### Claim 8 (depends on 1)

The method for manufacturing a powder according to claim 1, wherein a drying temperature and a period of time for drying in the drying step correspond to a flash point of the liquid additive.

### Claim 9

A method for manufacturing a powder comprising:
a mixing step in which a powder and a liquid additive are mixed together;
a drying step in which the powder mixed in the mixing step is dried;
a loading step in which the powder dried in the drying step is loaded into a pulverizer;
a supplying step in which a high-pressure gas is supplied to the pulverizer; and
a pulverizing step in which the powder is pulverized by the pulverizer.

### Claim 10 (depends on 9)

The method for manufacturing a powder according to claim 9, wherein the liquid additive is diethylene glycol monomethyl ether.

### Claim 11 (depends on 10)

The method for manufacturing a powder according to claim 10, wherein the powder is a powder including barium titanate.

### Claim 12 (depends on 11)

The method for manufacturing a powder according to claim 11, wherein a drying temperature and a period of time for drying in the drying step correspond to a flash point of the liquid additive.

### Claim 13 (depends on 10)

The method for manufacturing a powder according to claim 10, wherein a drying temperature and a period of time for drying in the drying step correspond to a flash point of the liquid additive.

### Claim 14 (depends on 9)

The method for manufacturing a powder according to claim 9, wherein the powder is a powder including barium titanate.

### Claim 15 (depends on 14)

The method for manufacturing a powder according to claim 14, wherein a drying temperature and a period of time for drying in the drying step correspond to a flash point of the liquid additive.

### Claim 16 (depends on 9)

The method for manufacturing a powder according to claim 9, wherein a drying temperature and a period of time for drying in the drying step correspond to a flash point of the liquid additive.
