Method for purifying a chlorine supply
AssigneeBASF SE
InventorsRobert A. Doerr, Steven D. Gagnon, Kenneth K. Bordelon, Johannes D. Jacobs, Thomas A. Grzanka
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AssigneeBASF SE
InventorsRobert A. Doerr, Steven D. Gagnon, Kenneth K. Bordelon, Johannes D. Jacobs, Thomas A. Grzanka
Estimating the term…
This invention provides a method for purifying a chlorine supply that includes a chlorine component, a bromine component, and nitrogen trichloride. The method includes the steps of introducing the chlorine supply into a vaporizer, heating the chlorine supply in the vaporizer to form a vapor, and introducing the vapor into a distillation system to provide purified chlorine gas, a distillate that includes liquid chlorine and the bromine component, and a bottoms component including the nitrogen trichloride. The method also includes the steps of condensing the vapor in a reflux condenser, heating the condensate in a reboiler, removing the purified chlorine gas from the distillation system, and removing the distillate from the distillation system.
A method of controlling a flow of vapor from a vaporizer to a distillation system comprising a distillation tower that has an upper end, a lower end, and a vapor-liquid contact device, a reflux condenser disposed above the distillation tower and in fluid communication with the upper end of the distillation tower to condense the vapor into a condensate such that the condensate flows into the upper end of the distillation tower, and a reboiler disposed below the distillation tower and in fluid communication with the lower end of the distillation tower to heat the condensate, wherein the reflux condenser, the reboiler, and a vapor input to the distillation tower are electronically coupled to a flow controlling device for controlling a rate of introducing the vapor into the distillation system, said method comprising the steps of:
A distillation system for purifying a chlorine supply comprising a chlorine component, a bromine component, and nitrogen trichloride, said distillation system forming purified chlorine gas having less than 20 parts by weight of said bromine component per one million parts by weight of said purified chlorine gas and forming a distillate comprising liquid chlorine and said bromine component, said system fluidly connected to a vaporizer and comprising:
Dependencies are inferred from the claim text.