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US 8,710,217 B2Granted
Method for producing lactamates by way of thin film evaporation
AssigneeRhein Chemie Rheinau GmbH
InventorsWilhelm Laufer, Hans Kasper, Stefan Schattner, Klaus Allgoewer, Bernd Kray, Michael Wuehr
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Abstract
A method is described for producing lactamates by reacting alcoholates with lactams, wherein a reaction mixture comprising at least one alcoholate and at least one lactam is subjected to thin film evaporation.
Claims13
A process for preparing a lactamate, comprising:
- (a) forming a reaction mixture comprising at least one alkoxide and at least one lactam by introducing the at least one lactam to the at least one alkoxide to obtain a reactant mixture wherein said lactam is ε-caprolactam;
- (b) homogenizing the reactant mixture at a temperature between 30° and 70° C. to obtain a homogenized reactant mixture wherein the homogenization results in essentially no reaction between the at least one alkoxide with the at least one lactam;
- (c) feeding the homogenized reactant mixture into a thin-film evaporator;
- (d) reactively distilling the reactant mixture fed in the thin-film evaporator at a temperature of 30 to 60° C., optionally with simultaneous stripping of the reactant mixture in countercurrent;
- and
- (e) obtaining the lactamate in the thin-film evaporator.
3 more elements
Dependencies are inferred from the claim text.