Process for preparing ammonic glyphosate granules
AssigneeSipcam S.P.A.
InventorsMarco Bernardini, Francesca Borgo, Luigi Capuzzi, Edoardo Russo
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Abstract
A process for preparing water-soluble granules of amnionic glyphosate comprising: a) addition of glyphosate acid to a Broensted base which supplies ammonium ions in a molar ratio base/acid comprised between 0.8 and 1.1; b) homogenization of the mixture prepared in a); c) addition of one or more surfactants in amounts in the range 5%-50% by weight based on the glyphosate acid; d) mixing of the mass prepared in c) for a time lower than about 10 minutes until obtaining an extrudable mass; e) extrusion of the mass obtained in d); f) drying until obtaining a granule having a residual moisture lower than 1%.
Claims13
A process for preparing water-soluble ammonic glyphosate granules comprising:
- a) addition of glyphosate acid, under wet cake form, to a solid Broensted base, which supplies ammonium ions, in amounts equal to a molar ratio base/acid between 0.8 and 1.1, optionally in the presence of coformulating agents;
- b) homogenization of the mixture prepared in a);
- c) addition of one or more surfactants, in a liquid form under stirring in amounts in the range 5%-50% by weight based on the glyphosate acid;
- d) mixing of the mass prepared in c) for a time lower than 10 minutes, until obtaining an extrudable mass wherein unreacted glyphosate acid, ammonium glyphosate and Broensted base are present;
- wherein, with respect to the initial acid amount, the unreacted glyphosate acid is present in an amount ranging from 70% to 10%, ammonic glyphosate is present a molar amount from 30% to 90%, and the corresponding amount of the unreacted base is present in the extrudable mass;
- e) extrusion by low pressure extruders of radial, basket or twin dome types of the mass obtained in d);
- f) drying until obtaining a granule having a residual moisture lower than 1% and completing salification of glyphosate.
Dependencies are inferred from the claim text.