# US 8,571,296 B2 · Method of testing the integrity of spiral wound modules

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- Number: US 8,571,296 B2
- Document ID: US8571296B2
- Status: Granted
- Kind: B2
- Application number: 12/903,236
- Filed: 2010-10-13
- Published: 2011-04-21
- Granted: 2013-10-29
- Earliest claimed: 2009-10-19
- Assignees: Dow Global Technologies LLC
- Applicants: Steven D. Jons
- Inventors: Steven D. Jons
- Web page: https://patentgrep.com/patent/US8571296B2

## CPC

- B01D 65/104: {Detection of leaks in membrane apparatus or modules}
- B01D 65/102: {Detection of leaks in membranes}
- Y02A 20/131: Reverse-osmosis
- B01D: SEPARATION (separating solids from solids by wet methods B03B, B03D; by pneumatic jigs or tables B03B; by other dry methods B07; magnetic or electrostatic separation of solid materials from solid materials or fluids, separation by high-voltage electric fields B03C; centrifuges, vortex apparatus B04; presses per se for squeezing-out liquid from liquid-containing material B30B9/02; treatment of water C02F, e.g. softening by ion-exchange C02F1/42; {arrangements of air intake cleaners in gas turbine plants F02C7/05} ; arrangements or mounting of filters in air-conditioning, air-humidification or ventilation F24F13/28)
- Y02A: TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE

## Abstract

Methods for testing the integrity of spiral wound modules including the introduction of pressurized gas within a sealed permeate collection tube and the detection of gas exiting at least one of the scroll faces of the module. The location(s) of gas exiting the scroll face can be correlated to defects in the module. In preferred embodiments, the subject test methods are non-destructive and can be applied to modules in either a dry or wet condition.

## Claims

### Claim 1

A method for testing the integrity of a spiral wound module conducted in a gaseous environment, wherein the module comprises: a permeate collection tube extending between two opposing ends and including a plurality of openings along its length, and at least one membrane envelope wound about the permeate collection tube and forming two opposing scroll faces, wherein the membrane envelope is in fluid communication with the openings along the permeate collection tube; wherein the method comprises the steps of:
sealing the opposing ends the permeate collection tube from the gaseous environment,
introducing a pressurized test gas into the permeate collection tube, and
detecting test gas exiting from at least one scroll face of the spiral wound module.

### Claim 2 (depends on 1)

The method of claim 1 wherein the step of detecting comprises obtaining an image of test gas exiting the scroll face of the spiral wound module.

### Claim 3 (depends on 2)

The method of claim 2 wherein the image of test gas exiting the scroll face of the spiral wound module is recorded by a camera.

### Claim 4 (depends on 3)

The method of claim 3 wherein the image is compared with a reference standard.

### Claim 5 (depends on 3)

The method of claim 3 wherein the test gas is detected by a camera sensitive to light of a wavelength within at least one of the following ranges: i) 3.5-4.6 microns and ii) 8-12 microns.

### Claim 6 (depends on 3)

The method of claim 3 wherein the step of detecting comprises illuminating the scroll face with light having wavelengths which are at least partially absorbed by the test gas while recording an image of test gas exiting the scroll face of the spiral wound module with a camera sensitive to such wavelengths.

### Claim 7 (depends on 1)

The method of claim 1 wherein the step of introducing a pressurized test gas into the permeate collection tube comprises introducing the test gas to a section of the permeate collection tube while simultaneously introducing a non-test gas to the remainder of the permeate collection tube.

### Claim 8 (depends on 1)

The method of claim 1 wherein the membrane envelope comprises a reverse osmosis or nanofiltration membrane.

### Claim 9 (depends on 1)

The method of claim 1 wherein the step of detecting comprises detecting test gas exiting one scroll face of the spiral wound module while simultaneously introducing a sweep gas to the opposite scroll face of the spiral wound module.

### Claim 10 (depends on 1)

The method of claim 1 wherein the spiral wound module is provided in a dry state.