# US 8,562,208 B2 · Critical temperature indicator > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 8,562,208 B2 - Document ID: US8562208B2 - Status: Granted - Kind: B2 - Application number: 13/301,082 - Filed: 2011-11-21 - Published: 2013-05-23 - Granted: 2013-10-22 - Earliest claimed: 2011-11-21 - Assignees: KLT Technologies - Applicants: Steven L. Yeager; T. Randall Lane - Inventors: Steven L. Yeager; T. Randall Lane - Web page: https://patentgrep.com/patent/US8562208B2 ## CPC - G01K 11/12: using changes in colour, translucency or reflectance - G01K: MEASURING TEMPERATURE; MEASURING QUANTITY OF HEAT; THERMALLY-SENSITIVE ELEMENTS NOT OTHERWISE PROVIDED FOR (radiation pyrometry G01J5/00) ## Abstract A temperature descending indicator which gives a visual indication when the indicator has been exposed to temperatures below a set threshold temperature includes a container having a translucent portion, a first temperature sensitive gel of a first color which will convert to liquid when it is exposed to temperatures below the set threshold temperature, and a second temperature sensitive gel of a second color which will convert to liquid when it is exposed to temperatures below the set threshold temperature, wherein the second temperature sensitive gel is disposed adjacent the translucent portion in a manner to obscure the visibility of the first temperature sensitive gel. A method of making the indicator includes disposing one color gel over the other. ## Claims ### Claim 1 A temperature descending indicator which gives a visual indication when the indicator has been exposed to temperatures below a set threshold temperature, which includes: a container having a translucent portion; a first temperature sensitive non-liquid of a first color which will convert to liquid when it is exposed to temperatures below the set threshold temperature; and a second temperature sensitive non-liquid of a second color which will convert to liquid when it is exposed to temperatures below the set threshold temperature, wherein said second temperature sensitive non-liquid is disposed adjacent said translucent portion in a manner to obscure the visibility of said first temperature sensitive non-liquid wherein said second temperature sensitive non-liquid includes a colorant of lesser density and said first temperature sensitive non-liquid includes a colorant of higher density and such that when said non-liquids convert to liquid, a permanent color change occurs from density shift of said colorants. ### Claim 2 (depends on 1) The temperature descending indicator of claim 1, said second temperature sensitive non-liquid is provided in greater volume than said first temperature sensitive non-liquid. ### Claim 3 (depends on 1) The temperature descending indicator of claim 1, wherein said second temperature sensitive non-liquid includes a red colorant and said first temperature sensitive non-liquid includes a green colorant. ### Claim 4 (depends on 3) The temperature descending indicator of claim 3, wherein said color change goes from green to red. ### Claim 5 (depends on 3) The temperature descending indicator of claim 3, wherein said second non-liquid includes from about 60-95% Base Sol-Gel, 0.25-5% Chromium Oxide Green Pigment and 5-35% Barium Sulfate Powder and said first non-liquid includes from about 80-98% Base Sol Gel, 2-20% and Pigment Red 2. ### Claim 6 (depends on 1) The temperature descending indicator of claim 1, wherein said temperature sensitive non-liquids include a sol-gel. ### Claim 7 (depends on 1) The temperature descending indicator of claim 1, wherein said container includes a translucent film and an opaque backing which sealably contains said non-liquids. ### Claim 8 (depends on 7) The temperature descending indicator of claim 7, wherein said film includes a laminate of PCTFE, Polychlorotrifluoroethylene, and polyvinylchloride. ### Claim 9 (depends on 7) The temperature descending indicator of claim 7, wherein said translucent film is a low moisture vapor transfer rate material. ### Claim 10 (depends on 1) The temperature descending indicator of claim 1, wherein said indicator is operable at temperatures as low as −10 degrees C. ### Claim 11 (depends on 1) The temperature descending indicator of claim 1, wherein said second temperature sensitive non-liquid includes additives giving said second temperature sensitive non-liquid a given density and said first temperature sensitive non-liquid includes additives giving said first temperature sensitive non-liquid one of a lower and a higher given density than said second temperature sensitive non-liquid. ### Claim 12 A method of forming a temperature indicator, which includes: providing a blister film container having a translucent portion, loading a first color temperature sensitive non-liquid that contains high density pigment into said blister film container in a position to cover said translucent portion wherein said first color temperature sensitive non-liquid will convert to liquid when it is exposed to temperatures below a set threshold temperature, loading a second color temperature sensitive non-liquid that contains lower density pigment into said blister film container adjacent said first color temperature sensitive non-liquid in a position such that only said first color temperature sensitive non-liquid is seen when viewing through said translucent portion and wherein said second color temperature sensitive non-liquid will convert to liquid when it is exposed to temperatures below the set threshold temperature and such that when said non-liquids convert to liquid, a permanent color change occurs from density shift of said colorants, and providing a backing onto said container to seal said temperature sensitive non-liquids in their positions. ### Claim 13 (depends on 12) The method of claim 12, wherein said non-liquids are sensitive to a descending temperature rendering said non-liquids liquid. ### Claim 14 (depends on 12) The method of claim 12, wherein said backing is opaque. ### Claim 15 (depends on 12) The method of claim 12, wherein said temperature sensitive non-liquids include a sol-gel. ### Claim 16 (depends on 12) The method of claim 12, wherein said indicator is constructed of low MVTR translucent polymer film and opaque backing to form a package with low MVTR and long shelf life.