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US 8,461,071 B2Granted
Polycrystalline group III metal nitride with getter and method of making
AssigneeSoraa, Inc.
InventorMark P. D'Evelyn
Life of this patent
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Abstract
A gettered polycrystalline group III metal nitride is formed by heating a group III metal with an added getter in a nitrogen-containing gas. Most of the residual oxygen in the gettered polycrystalline nitride is chemically bound by the getter. The gettered polycrystalline group III metal nitride is useful as a raw material for ammonothermal growth of bulk group III nitride crystals.
Claims18
A polycrystalline gallium-containing group III metal nitride material, comprising:
- a plurality of grains of a crystalline gallium-containing group III metal nitride;
- the plurality of grains having an average grain size in a range of from about 10 nanometers to about 1 millimeter and defining a plurality of grain boundaries;
- and
- the crystalline gallium-containing group III metal nitride having:
- an atomic fraction of a gallium-containing group III metal in a range of from about 0.49 to about 0.55, the metal being selected from at least one of aluminum, indium, and gallium;
- and
- an oxygen content in the form of a gallium-containing group III metal oxide or a substitutional impurity within the crystalline gallium-containing group III metal nitride less than about 10 parts per million (ppm);
- and
- a plurality of inclusions within at least one of the plurality of grain boundaries and the plurality of grains, the plurality of inclusions comprising a getter, the getter constituting a distinct phase from the crystalline gallium-containing group III metal nitride and being incorporated into the polycrystalline gallium-containing group III metal nitride material at a level greater than about 200 parts per million.
6 more elements
Dependencies are inferred from the claim text.