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US 8,409,540 B2Granted
Process for preparing hydrotalcite
AssigneeOh Young Kwon
InventorsOh Young Kwon, Im Sun Her
Life of this patent
Estimating the term…
Abstract
Disclosed is a method of preparing hydrotalcite having superior anion exchange capability and heat stability by forming a seed so that CO32− ions are located to be maximally stable between Mg—Al layers and then conducting primary crystallization and secondary crystallization.
Claims8
A method of preparing hydrotalcite, comprising:
- 1) mixing a magnesium source, an aluminum source, a carbonate ion source, and an alkali source, thus preparing a mixture, and then stirring the mixture at 30˜80° C. for 3˜4 hours, thus forming a seed;
- 2) adding an alkali source to the seed, increasing a temperature to 90˜150° C., and then performing a reaction for 1˜12 hours while maintaining the temperature of 90˜150° C., thus obtaining primarily crystallized hydrotalcite particles;
- 3) adding a magnesium source, an aluminum source and a carbonate ion source to the primarily crystallized hydrotalcite particles, and then performing a reaction at 90˜150° C. for 1˜18 hours, thus obtaining secondarily crystallized hydrotalcite particles;
- and
- 4) washing the secondarily crystallized hydrotalcite particles with distilled water and then performing drying.
2 more elements
Dependencies are inferred from the claim text.