# US 8,273,156 B2 · Method and apparatus for water distillation and recovery

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- Number: US 8,273,156 B2
- Document ID: US8273156B2
- Status: Granted
- Kind: B2
- Application number: 12/496,411
- Filed: 2009-07-01
- Published: 2010-01-07
- Granted: 2012-09-25
- Earliest claimed: 2008-07-01
- Inventors: Eric John Dole
- Web page: https://patentgrep.com/patent/US8273156B2

## CPC

- B01D 1/0017: {Use of electrical or wave energy (B01D1/0029 takes precedence)}
- B01D 3/06: Flash distillation
- B01D 3/10: Vacuum distillation (B01D3/12 takes precedence)
- C02F 1/06: Flash evaporation
- C02F 1/441: {by reverse osmosis}
- C02F 1/46: by electrochemical methods
- C02F 2101/103: {Arsenic compounds}
- C02F 2101/14: Fluorine or fluorine-containing compounds
- C02F 2201/009: Apparatus with independent power supply, e.g. solar cells, windpower or fuel cells
- C02F 2209/005: Processes using a programmable logic controller [PLC]
- C02F 2209/42: Liquid level
- C02F 2301/063: Underpressure, vacuum
- Y02A 20/212: Solar-powered wastewater sewage treatment, e.g. spray evaporation
- Y02W 10/37: using solar energy
- B01D: SEPARATION (separating solids from solids by wet methods B03B, B03D; by pneumatic jigs or tables B03B; by other dry methods B07; magnetic or electrostatic separation of solid materials from solid materials or fluids, separation by high-voltage electric fields B03C; centrifuges, vortex apparatus B04; presses per se for squeezing-out liquid from liquid-containing material B30B9/02; treatment of water C02F, e.g. softening by ion-exchange C02F1/42; {arrangements of air intake cleaners in gas turbine plants F02C7/05} ; arrangements or mounting of filters in air-conditioning, air-humidification or ventilation F24F13/28)
- C02F: TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE (separation in general B01D; special arrangements on waterborne vessels of installations for treating water, waste water or sewage, e.g. for producing fresh water, B63J; adding materials to water to prevent corrosion C23F; treating radioactively-contaminated liquids G21F9/04; regeneration of reactants for recirculation into processes, see the relevant places for the processes)
- Y02A: TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02W: CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT

## Abstract

Contaminated water stored in an equalization basin is distributed to one or more flash vessels and a desired vacuum is pulled in a filled flash vessel, reducing the boiling point of the contained contaminated water. The suction force is preferably created by passing the contaminated water under pressure through a differential pressure injector. The contaminated water in the flash vessel completes an electrical circuit between conductive plates and a heating element that are submerged therein. An alternating electrical current is applied, some of which is conducted by the contaminated water to a heating element that heats the water, and the rest of which dissipates as thermal energy, heating the contaminated water. The alternating current is preferably generated by passing the contaminated water under pressure through a hydroelectric power generator. Little thermal energy is needed to evaporate the contaminated water, which condenses at the top of the flash vessel and is collected from a collection trough. Slurry created by distillation is delivered to the equalization basin to increase the conductivity and temperature of the stored contaminated water.

## Claims

### Claim 1

A method of distilling contaminated water, the method comprising:
a. filling a flash vessel with a predetermined volume of contaminated water;
b. pulling a vacuum in the flash vessel, wherein pulling the vacuum comprises delivering a stream of the contaminated water under pressure to an injector connected to the flash vessel; and
c. passing an electrical current through the contaminated water in the flash vessel to cause a phase change of the contaminated water into evaporated water;
wherein the injector is connected to the flash vessel at the bottom of the flash vessel so that the vacuum may be continuously pulled without evacuating evaporated water from the flash vessel.

### Claim 2 (depends on 1)

The method of claim 1 wherein the injector is a Venturi-type differential pressure injector.

### Claim 3

A method of distilling contaminated water, the method comprising:
a. filling a flash vessel with a predetermined volume of contaminated water;
b. pulling a vacuum in the flash vessel;
c. generating an electrical current by delivering the contaminated water under pressure to a power generator; and
d. passing the electrical current through the contaminated water in the flash vessel to cause a phase change of the contaminated water into evaporated water.

### Claim 4

A method of distilling contaminated water, the method comprising:
a. filling a flash vessel with a predetermined volume of contaminated water, the flash vessel being filled from an equalization basin;
b. pulling a vacuum in the flash vessel;
c. passing an electrical current through the contaminated water in the flash vessel to cause a phase change of the contaminated water into evaporated water;
d. repeating steps b and c until a desired amount of distilled water is collected and a slurry remains in the flash vessel; and
e. delivering the slurry to the equalization basin to increase the temperature and conductivity of stored contaminated water in the equalization basin.

### Claim 5

A method of distilling contaminated water, the method comprising:
a. filling a flash vessel with a predetermined volume of contaminated water, the flash vessel comprising a flash chamber and a condensing chamber separated by one or more thermally non-conductive flanges;
b. pulling a vacuum in the flash vessel;
c. passing an electrical current through the contaminated water in the flash vessel to cause a phase change of the contaminated water into evaporated water; and
d. cooling one or more surfaces of the condensing chamber to facilitate condensation of the evaporated water the cooling comprising delivering the contaminated water to a heat sink bath surrounding the condensing chamber.

### Claim 6 (depends on 5)

The method of claim 5 wherein the contaminated water is delivered to the heat sink bath under pressure and on a path that is non-radial to the heat sink bath, such that the delivery creates a whirlpool effect in the heat sink bath.

### Claim 7

A method of recovering distilled water from a high pressure concentrate stream, the method comprising:
a. generating electrical power by passing at least a portion of the concentrate stream through a hydroelectric power generator;
b. passing at least a portion of the concentrate stream through an injector connected to a flash vessel;
c. delivering at least a portion of the concentrate stream into a heat sink bath surrounding a portion of the flash vessel;
d. delivering the concentrate stream, including the portions from the generator, injector, and heat sink bath, to an equalization basin configured to distribute contaminated water from the concentrate stream to the flash vessel;
e. filling the flash vessel with a predetermined volume of contaminated water from the equalization basin;
f. sealing the flash vessel after it has been filled;
g. pulling a vacuum in the flash vessel with the injector;
h. heating the volume of contaminated water to a depressed boiling point, the heating comprising passing an alternating current through the volume of contaminated water to an electrical load;
i. collecting a predetermined volume of distilled water from the flash vessel; and
j. removing a slurry from the flash vessel.

### Claim 8 (depends on 7)

The method of claim 7 wherein the generator is a micro-turbine.

### Claim 9 (depends on 7)

The method of claim 7 wherein the flash vessel comprises:
a. a condensing chamber comprising the portion of the flash vessel surrounded by the heat sink bath;
b. a flash chamber positioned below the condensing chamber and configured to contain the volume of contaminated water;
c. an internal vent connecting the flash chamber to the condensing chamber so that evaporated water may rise from the flash chamber into the condensing chamber; and
d. first and second conducting plates positioned to be at least partially submerged in the volume of contaminated water, the first conducting plate being in electrical communication with the generator and the second conducting plate being in electrical communication with the electrical load;
and wherein passing the alternating current through the volume of contaminated water to the electrical load comprises passing the alternating current from the first conducting plate through the volume of contaminated water to the second conducting plate.

### Claim 10 (depends on 9)

The method of claim 9 wherein the internal vent is a standpipe extending substantially into the condensing chamber, the standpipe defining the maximum fill volume of a distilled water collection trough.

### Claim 11 (depends on 9)

The method of claim 9 wherein the electrical load comprises a heating element positioned at least partially within the flash chamber, and wherein heating the volume of contaminated water further comprises powering the heating element with the alternating current.

### Claim 12 (depends on 9)

The method of claim 9 wherein the flash vessel further comprises a flow port through the bottom of the flash chamber, the flow port being connected to the injector so that the vacuum is pulled through the flow port.

### Claim 13 (depends on 7)

The method of claim 7 wherein the heating further comprises sealing the equalization basin with a non-permeable hood so that stored contaminated water is heated by a greenhouse effect.

### Claim 14 (depends on 7)

The method of claim 7 wherein the heating further comprises passing the predetermined volume of contaminated water through a water heater powered by the generator before the flash vessel is filled.

### Claim 15

A water recovery apparatus comprising:
a. an equalization (“EQ”) basin for storing incoming contaminated water, the equalization basin comprising:
i. a non-permeable hood that creates a substantially airtight seal over the contaminated water;
ii. an EQ air valve attached to the hood to allow rising and falling of the level of contaminated water when the EQ air valve is open; and
iii. an equalization basin collecting trough positioned below the hood to collect distilled water that condenses on the hood;
b. a hydroelectric power generator configured to receive a first stream of contaminated water under pressure, generate power from the contaminated water, and deliver the first stream of contaminated water to the equalization basin;
c. a Venturi-type differential pressure injector comprising a vacuum port and configured to receive a second stream of contaminated water under pressure, generate a suction force at the vacuum port, and output a discharge stream of contaminated water;
d. a slurry pump configured to deliver slurry to the equalization basin;
e. one or more flash vessels configured to receive a predetermined volume of contaminated water from the equalization basin, the flash vessels comprising:
i. a condensing chamber comprising a distilled water collection trough;
ii. a flash chamber positioned below the condensing chamber and configured to contain the volume of contaminated water;
iii. at least one chamber flange separating the condensing chamber and the flash chamber;
iv. a standpipe extending through each chamber flange and connecting the flash chamber to the condensing chamber so that evaporated water may rise from the flash chamber into the condensing chamber;
v. an air valve attached to the condensing chamber to allow filling and emptying of the flash vessel;
vi. a heating element positioned within the flash chamber to be submerged in the volume of contaminated water;
vii. first and second conducting plates positioned within the flash chamber to be at least partially submerged in the volume of contaminated water, the first conducting plate being in electrical communication with the generator and the second conducting plate being in electrical communication with the heating element; and
viii. a flow port through the bottom of the flash chamber, the flow port being connected to each of:
1. the equalization basin, to allow filling of the flash chamber;
2. the vacuum port of the pressure differential injector, to allow a vacuum to be pulled in the flash vessel without evacuating evaporated water; and
3. the slurry pump, to allow removal of the slurry;
f. a fill valve positioned in the connection between the flow port and the equalization basin;
g. a vacuum valve positioned in the connection between the flow port and the vacuum port of the pressure differential injector;
h. a slurry valve positioned in the connection between the flow port and the slurry pump;
i. a distilled water drain valve positioned to allow collection of distilled water from the distilled water collection trough;
j. a heat sink bath surrounding the condensing chamber and configured to receive a third stream of contaminated water and deliver a bath overflow to the equalization basin; and
k. a programmable logic controller powered by the generator and configured to control the processes of filling the flash vessel, pulling a vacuum, heating the contaminated water, collecting the distilled water from the flash vessel, and removing slurry from the flash vessel, by opening or closing each of the fill vale, vacuum valve, slurry valve, air valve, and distilled water drain valve, according to each process.

### Claim 16 (depends on 15)

The apparatus of claim 15 further comprising:
a. a fill pump positioned in the connection between the flow port and the equalization basin and configured to pump the volume of contaminated water into the flash vessel;
b. a water heater connected to the fill pump and configured to heat the volume of contaminated water; and
c. a cooling device configured to receive the third stream of contaminated water and deliver it to the heat sink bath.