Apparatus and process for preparing silanes
AssigneeEvonik Degussa GmbH
InventorsRaymund Sonnenschein, Peter Adler, Tim Pöpken, John Kahsnitz
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Abstract
Provided is an apparatus for preparing silanes of the general formula HnSiCU n where n=1, 2, 3 and/or 4 by dismutation of a chlorinated silane in the presence of a catalyst, wherein the apparatus includes: a distillation column having a column bottom, a column top, at least one feed inlet, a plurality of product offtakes, and a chimney tray; and a side reactor containing a catalyst bed having an upper edge, the side reactor being connected to the distillation column via at least three pipes including a first pipe, a second pipe, and a third pipe.
Claims22
An apparatus for preparing silanes of the general formula HnSiCl4, where n=1, 2, 3 and/or 4 by dismutation of at least one chlorinated silane in the presence of a catalyst, wherein said apparatus comprises:
- at least one distillation column comprising a column bottom, a column top, at least one feed inlet, a plurality of product offtakes, and at least one chimney tray;
- and
- at least one side reactor comprising a catalyst bed having an upper edge, the side reactor being connected to the distillation column via at least three pipes comprising a first pipe, a second pipe, and a third pipe,
- wherein the side reactor, the catalyst bed, the first pipe, the second pipe, and the third pipe are positioned in relation to the chimney tray and the distillation column,
- the first pipe is connected to the distillation column at a position higher than the upper edge of the catalyst bed to discharge a condensate from the chimney tray into the catalyst bed,
- the first pipe comprises a branch pipe which has an opening in the distillation column at a position below the chimney tray and is configured to regulate a flow of the condensate,
- the second pipe is connected to the distillation column at a position below the chimney tray and the upper edge of the catalyst bed to discharge a liquid phase from the side reactor to the distillation column, and
- the third pipe is connected to the distillation column at a position higher than the chimney tray to discharge a gas phase from the side reactor to the distillation column.
Dependencies are inferred from the claim text.