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US 8,026,329 B2Granted
Polycarbosilane and method of producing the same
AssigneeTokai Carbon Korea Co., Ltd
InventorsYoung Hee Kim, Soo Ryong Kim, Woo Teck Kwon, Jung Hyun Lee
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Abstract
Provided are polycarbosilane and a method of producing the same. The polycarbosilane contains an allyl group, and thus can be cured by UV absorption when not exposed to the air.
Claims4
A method of producing polycarbosilane, comprising:
- dispersing metal sodium in an organic solvent;
- pre-mixing an allylmethyldichlorosilane monomer with a phenylmethyldichlorosilane monomer, and injecting the mixed monomer solution into the solution in which the metal sodium is dispersed;
- polymerizing polyallylphenylsilane by reaction of the mixed solution of the monomers and the metal sodium at 90 to 130° C.;
- separating a precipitate of the polymerized polyallylphenylsilane;
- performing a first conversion reaction on the separated polyallylphenylsilane precipitate under 5 to 30 atm at 300 to 370° C. for 5 to 20 hours;
- and
- performing a second conversion reaction on the resulting product under 5 to 30 atm at 400 to 470° C. for 5 to 20 hours,
- wherein the operations are performed in an inert gas atmosphere.
5 more elements
Dependencies are inferred from the claim text.