Low solids, high viscosity fabric softener compositions and process for making the same
AssigneeStepan Company
InventorsBranko Sajic, Xue Min Dong, Carmen Matache, Christopher A. Gariepy
Life of this patent
Estimating the term…
Abstract
Disclosed are low solids and high viscosity fabric softener compositions and processes for preparing them. The composition contains from about 0.05% to about 10% by weight of a rheology modifying fabric softening active comprising at least one long chain amine of the present technology, a derivative thereof, or a mixture thereof, and from about 1% to 10% by weight of an additional fabric softening active dispersed in water.
Claims11
A process for making a fabric softener composition, comprising the steps of:
- adding a rheology modifying fabric softening active comprising a long chain amine, a derivative thereof, or a mixture thereof to water at a temperature of between about 25° C. and about 70° C. to form a mixture, wherein the long chain amine has a general chemical structure of:
- wherein, R0 has a structure of R1—A—R2, where R1 is a C5-30 alkyl, alkylene, or alkenyl group, A is
- or
- where R5 is a C1-6 alkyl or alkylene group, a hydrogen, or a polyamine, R2 is a C1-6 alkylene group, a C1-30 alkoxylated group, or a covalent bond, and R3 or R4 independently is the same as R1—A—R2, a C1-5 alkyl group, or a hydrogen;
- adding a quaternary amine fabric softening active to the mixture at a temperature of between about 25° C. and about 70° C;
- cooling the mixture to a temperature at about 10° C. below to about 10° C. above the re-crystallization/solidification phase transition temperature of the dispersed fabric softening active or actives;
- and
- in-situ adjusting the pH of the long chain amine, derivative thereof or mixtures thereof and the quaternary amine fabric softening active to a pH in the range of about 1.5 to about 7.0 by adding a polyprotic acid at about or under the re-crystallization/solidification phase transition temperature of the fabric softening active or actives to form the fabric softener composition.
A process for making a fabric softener composition, comprising the steps of:
- making a concentrated pre-mix by adding a quaternary amine fabric softening active and a rheology modifying fabric softening active comprising a long chain amine, a derivative thereof, or a mixture thereof to water at a temperature of between about 35° C. and about 70° C. to form a homogeneous mixture, wherein the long chain amine has a general chemical structure of:
- wherein, R0 has a structure of R1—A—R2, where R1 is a C5-30 alkyl, alkylene, or alkenyl group, A is
- or
- where R5 is a C1-6 alkyl or alkylene group, a hydrogen, or a polyamine, R2 is a C1-6 alkylene group, a C1-30 alkoxylated group, or a covalent bond, and R3 or R4 independently is the same as R1—A—R2, a C1-5 alkyl group, or a hydrogen;
- cooling of the mixture to a temperature at about 10° C. below to about 10° C. above the re-crystallization/solidification phase transition temperature by the addition of a sufficient amount of cold water to dilute the mixture to a predetermined lower active concentration;
- in-situ adjusting the pH of the long chain amine, derivative thereof or mixtures thereof and the quaternary amine fabric softening active to a pH in the range of about 1.5 to about 7.0 by adding a polyprotic acid at about or under the re-crystallization/solidification phase transition temperature of the fabric softening active or actives to form the fabric softener composition.
Dependencies are inferred from the claim text.