Back to results
US 7,842,653 B2Granted
Process for the preparation of lubricants
AssigneeCouncil of Scientific and Industrial Research
InventorsSrinivas Darbha, Rajendra Srivastava, Paul Ratnasamy
Life of this patent
Estimating the term…
Abstract
The present invention provides an improved process for the preparation of lubricants from vegetable oil or fat obtained from animal source. The present invention involves a reaction of vegetable oil or fat with an alcohol in the presence of a double metal cyanide catalyst, at a temperature in the range of 150° to 200° C. for a period of 3-6 hrs to obtain the desired bio-lubricant.
Claims7
An improved process for the preparation of lubricants-comprising:
- a) dissolving a vegetative oil or fat in an alcohol,
- b) mixing the above said solution obtained in step(a) with a double metal cyanide catalyst that remains insoluble in the obtained mixture, followed by stifling, at a temperature in the range of 150° to 200° C., for a period of 3-6 hrs,
- c) cooling the above said reaction mixture to a temperature of about 25° C.,
- d) separating the catalyst from the above said reaction mixture
- e) removing the unreacted alcohol by distillation;
- and
- f) separation of glycerol by-products by adding petroleum ether and methanol to obtain the desired esterified product.
- wherein the conversion of oil to lubricant is in the range of 90.0-96.0 mol %.
5 more elements
Dependencies are inferred from the claim text.