Process for large-scale production of monodisperse nanoparticles
AssigneeSeoul National University Industry Foundation
InventorsTaeg-Hwan Hyeon, Jong-Nam Park
Life of this patent
Estimating the term…
Abstract
The present invention is directed to a process for making nanoparticles of metals, metal alloys, metal oxides and multi-metallic oxides, which comprises the steps of reacting a metal salt dissolved in water with an alkali metal salt of C4-25 carboxylic acid dissolved in a first solvent selected from the group consisting of C5-10 aliphatic hydrocarbon and C6-10 aromatic hydrocarbon to form a metal carboxylate complex; and heating the metal carboxylate complex dissolved in a second solvent selected from the group consisting of C6-25 aromatic, C6-25 ether, C6-25 aliphatic hydrocarbon and C6-25 amine to produce the nanoparticles.
Claims12
A process for making nanoparticles of metals, metal oxides and multi-metallic oxides, which comprises the steps of:
- i) reacting a metal salt dissolved in water with an alkali metal salt of C4-25 carboxylic acid dissolved in a first solvent selected from the group consisting of C5-10 aliphatic hydrocarbon and C6-10 aromatic hydrocarbon to form a metal carboxylate complex;
- ii) separating said metal carboxylate complex from an upper organic layer containing said metal carboxylate complex by removing said first solvent;
- and
- iii) heating said metal carboxylate complex dissolved in a second solvent selected from the group consisting of C6-25 aromatic, C6-25 ether, C6-25 aliphatic hydrocarbon and C6-25 amine at a rate of 1° C./min to 200° C./min from room temperature to the boiling temperature of said second solvent to cause an abrupt thermal decomposition of said metal carboxylate complex and instantaneous nucleation of monodisperse nanoparticles, to produce the monodisperse nanoparticles.
Dependencies are inferred from the claim text.