# US 7,746,465 B2 · Sample holder for an optical element

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- Number: US 7,746,465 B2
- Document ID: US7746465B2
- Status: Granted
- Kind: B2
- Application number: 11/966,557
- Filed: 2007-12-28
- Published: 2008-07-24
- Granted: 2010-06-29
- Earliest claimed: 2007-01-18
- Assignees: Hinds Instruments, Inc.
- Inventors: Douglas C. Mark
- Web page: https://patentgrep.com/patent/US7746465B2

## CPC

- G01N 21/23: Bi-refringence
- G01N 21/01: Arrangements or apparatus for facilitating the optical investigation
- G01N 2021/0339: {Holders for solids, powders}
- G01N 2201/02: Mechanical
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)

## Abstract

The sample holder includes support having a thickness and an aperture through the thickness of the support. A tilt mechanism is connected to the support for controlled tilting of the support, and the aperture through the support is configured to have a diameter that increases in a direction through the thickness of the support. This arrangement enables a light beam to pass through the same given area of the sample, irrespective of whether the sample is held perpendicular to the beam or held at a tilted position relative to the beam. In one embodiment, the holder includes an efficient magnetic clamp mechanism for securing the sample to the holder. The holder compactly integrates with tilting mechanisms a sample rotation mechanism.

## Claims

### Claim 1

A sample holder comprising:
a support having a thickness and an aperture through the thickness of the support;
a tilt mechanism connected to the support for controlled tilting of the support; and
wherein the aperture through the support is configured to have a diameter that increases in a direction through the thickness of the support.

### Claim 2 (depends on 1)

The holder of claim 1 wherein the aperture defines a frustum shape in the support.

### Claim 3 (depends on 1)

The holder of claim 1 wherein the tilt mechanism is configured to permit tilting of the sample by a maximum amount corresponding to a first angle and;
wherein the support has a planar surface and the diameter of the aperture defines a sidewall that is inclined relative to that surface by a second angle the second angle being equal to or less than the complement of the first angle.

### Claim 4 (depends on 1)

The holder of claim 1 wherein the tilt mechanism provides for rotation of the support about a first axis, the holder including a mechanism for rotating the support about a second axis that is normal to the first axis.

### Claim 5 (depends on 1)

The holder of claim 1 wherein the tilt mechanism includes separate gross tilt angle adjustment and fine tilt angle adjustment.

### Claim 6 (depends on 1)

The holder of claim 1 including opposing axle members for rotationally mounting the support at opposing edges thereof.

### Claim 7 (depends on 6)

The holder of claim 6 including both a gross tilt angle adjustment mechanism and a separate fine tilt angle adjustment mechanism connected to one of the axle members.

### Claim 8 (depends on 5)

The holder of claim 5 wherein the fine tilt angle adjustment is selectively disengageable to remove resistance to gross tilt adjustment.

### Claim 9 (depends on 1)

The holder of claim 1 including a magnetic clamp for holding a sample to the sample holder.

### Claim 10 (depends on 4)

The holder of claim 4 wherein the holder includes a frame that encloses a worm and the support includes a worm wheel mounted thereto to engage the worm, thereby forming a worm gear mechanism for rotating the support about the second axis.

### Claim 11 (depends on 1)

The holder of claim 1 further comprising a frame supported by opposing hubs, both hubs comprising detent mechanisms to releasable secure the sample support in a selected tilt position.

### Claim 12

A method of supporting an optical sample in the path of a light beam so that the sample may be oriented at any selected one of a plurality of orientations relative to the light beam such that the beam path is oblique to the surface of the sample, the method comprising the step of supporting the sample in a holder that has a frustum shaped aperture therethrough and that can be selectively tilted about an axis that is perpendicular to the beam path.

### Claim 13 (depends on 12)

The method of claim 12 including the step of magnetically clamping the optical sample to the holder.

### Claim 14 (depends on 12)

The method of claim 12 including the step of mounting the sample for rotation within the holder.

### Claim 15

A sample support comprising:
a holder having a frame and a frustum shaped aperture therethrough;
opposing hub assemblies for supporting the frame about opposing axle members that permit tilting of the holder;
tilting means for enabling precise selection of a tilt position of the frame about a tilt axis; and
detent means for securing the frame in the tilt position.

### Claim 16 (depends on 15)

The support of claim 15 wherein the tilting means comprises separate gross and fine adjustment means for respective gross and fine adjustment of the frame into the tilt position.

### Claim 17 (depends on 15)

The support of claim 15 including a rotatable member secured to the frame for supporting the optical sample in a manner that permits rotation about an axis that is perpendicular to the tilt axis.

### Claim 18 (depends on 15)

The holder of claim 15 including a magnetic clamp for securing a sample to the holder.
