Back to results
US 7,731,879 B2Granted
Extrusion of peroxide crosslinkable polymer parts
AssigneeRehau AG & Co.
InventorsKarlheinz Winter, Gerhard Dunkel, Günther Seewald, Hermann Zwilling
Life of this patent
Estimating the term…
Abstract
A process for the extrusion of peroxide crosslinked polymer parts, mainly tubes, in which the crosslinkable polymer is heated in an extruder in a controlled manner to a value above the crystallite melting point of the polymer, but below the crosslinking temperature, and fed continuously to an extrusion die to create the part and in which at least a partial crosslinking of the polymer is achieved in the extrusion die by heating of the polymer above a crosslinking temperature provision.
Claims13
A method for extruding a peroxide crosslinked polymer tube, comprising:
- supplying a mixture to a screw extruder, the mixture comprising:
- a crosslinkable polymer, a crosslinking agent, and a stabilizing agent, wherein the polymer has a crystallite melting point and a crosslinking temperature, and wherein the screw extruder is a conically tapered screw extruder having at least two sections of differing spiral pitch;
- heating the mixture in the screw extruder with an external heating unit to a temperature above the crystallite melting point but below the crosslinking temperature;
- controlling the temperature of the mixture in the screw extruder with the external heating unit and an internal cooling unit;
- continuously feeding the mixture from the screw extruder to an extrusion die, wherein a melting pressure before entry to the extrusion die is approximately 700-1500 bar;
- heating the mixture in the extrusion die above the crosslinking temperature to effect at least a partial crosslinking of the polymer in the extrusion die, wherein the temperature (° C.) of the mixture in the extrusion die is at least 15% above the crosslinking temperature (° C.);
- and
- discharging the mixture from the extrusion die, wherein the degree of crosslinking of the polymer on discharge from the extrusion die is above 60%.
5 more elements
Dependencies are inferred from the claim text.