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US 7,678,358 B2Granted
Carbon fibers from kraft softwood lignin
AssigneeWeyerhaeuser NR Company
InventorsRobert C Eckert, Zia Abdullah
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Abstract
A method of making a carbon fiber from softwood alkaline black liquor lignin by acetylating the lignin to provide a meltable and drawable lignin.
Claims12
The process of forming a carbon fiber from kraft softwood lignin comprising:
- a) acetylating lignin obtained from softwood alkaline black liquor to provide a lignin acetate until the acetyl content of the dry lignin acetate is between 16% and 22% by weight as measured by deacetylation in alkali followed by ion chromatography wherein the lignin acetate melts when heated
- b) melt extruding the acetylated softwood acetylated lignin to provide a coherent “green” lignin fiber
- c) thermally stabilizing the melt extruded green lignin acetate fiber to a state that does not melt on subsequent heating
- d) carbonizing thermally stabilized softwood lignin acetate fiber.
1 more element
Dependencies are inferred from the claim text.