Blue dye with particularly high purity and positive triboelectric control effect
AssigneeClariant Produkte (Deutschland) GmbH
InventorsEduard Michel, Ruediger Baur, Hans-Tobias Macholdt, Norbert Kohl
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Abstract
A dye base sulfate and method of making are described. The dye base sulphate of formula (I) is produced with a residual amine content of less than 2000 ppm, as determined by HPLC, by precipitation of the dye base, made by Friedel-Crafts alkylation, substitution and hydrolysis, as the dye base sulphate is a) taken up in water and subjected to a first steam distillation then filtered and optionally dried at 50 to 180° C., b) the pressed cake is treated with water or the optionally dried dye base sulphate is moistened with water, c) subjected to a further steam distillation and filtration and d) dried at 50 to 180° C.
Claims9
A composition comprising a compound of formula (1)
- and an aniline, wherein the aniline is present in an amount less than 2000 ppm as determined by high performance liquid chromatography.
Dependencies are inferred from the claim text.