# US 7,610,768 B2 · Apparatus and methods for water regeneration from waste > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 7,610,768 B2 - Document ID: US7610768B2 - Status: Granted - Kind: B2 - Application number: 11/271,674 - Filed: 2005-11-09 - Published: 2007-05-10 - Granted: 2009-11-03 - Earliest claimed: 2005-11-09 - Assignees: Honeywell International Inc. - Inventors: Alex M. Lubman; Allen K. MacKnight; Volodimir G. Rifert; Ivan V. Zolotukhin; Vladimir I. Usenko; Petr A. Barabash; Aleksandr P. Strikun - Web page: https://patentgrep.com/patent/US7610768B2 ## CPC - B01D 3/08: in rotating vessels; Atomisation on rotating discs ({B01D1/222} , B01D3/10 take precedence) - B01D 3/10: Vacuum distillation (B01D3/12 takes precedence) - C02F 1/048: {Purification of waste water by evaporation} - Y02W 10/37: using solar energy - B01D: SEPARATION (separating solids from solids by wet methods B03B, B03D; by pneumatic jigs or tables B03B; by other dry methods B07; magnetic or electrostatic separation of solid materials from solid materials or fluids, separation by high-voltage electric fields B03C; centrifuges, vortex apparatus B04; presses per se for squeezing-out liquid from liquid-containing material B30B9/02; treatment of water C02F, e.g. softening by ion-exchange C02F1/42; {arrangements of air intake cleaners in gas turbine plants F02C7/05} ; arrangements or mounting of filters in air-conditioning, air-humidification or ventilation F24F13/28) - C02F: TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE (separation in general B01D; special arrangements on waterborne vessels of installations for treating water, waste water or sewage, e.g. for producing fresh water, B63J; adding materials to water to prevent corrosion C23F; treating radioactively-contaminated liquids G21F9/04; regeneration of reactants for recirculation into processes, see the relevant places for the processes) - Y02W: CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT ## Abstract A rotary multi-stage distiller for recovery of water from wastewater is provided. The rotary multi-stage distiller of the present invention can recover water from a wide variety of aqueous wastewaters such as, but not limited to, urine, condensate from air conditioning systems, wash water containing foaming soaps, seawater or polluted water. The multi-stage distiller can operate under vacuum conditions permitting the distillation to occur at low temperatures. The multi-stage distiller uses centrifugal forces for fluid pumping and for vapor/liquid separation. The multi-stage distiller comprises hydraulic seals for each stage which eliminate contamination of clean, recovered water by condensed waste water during the regeneration process. The multi-stage distiller also comprises a stationary shaft of stacked segments where each segment is associated with an individual stage of the multi-stage distiller. The number of stages therefore, of the multi-stage distiller of the present invention can be readily adjusted as needed by either adding a segment with a stage to the stationary shaft or removing a segment of the shaft with a stage to decrease the number of stages. ## Claims ### Claim 1 A multi-stage vacuum cascade distiller comprising: a housing; a cylindrical rotor cover disposed within the housing, the cylindrical rotor cover comprising an axis of rotation; a stationary shaft disposed within the cylindrical rotor cover, the stationary shaft comprising individual removable shaft sections wherein each shaft section comprises a stage of the multi-stage vacuum distiller; wherein each stage comprises heat exchange surfaces, partitions, an evaporation zone and a condensation zone; each of said partitions comprises a first opening proximate said stationary shaft and a second opening proximate said housing; and said first and said second openings being configured to discharge non-condensable gases. ### Claim 2 (depends on 1) The cascade distiller of claim 1 further comprising transportation channels in the stationary shaft, wherein the transportation channels comprise passages drilled into the stationary shaft. ### Claim 3 (depends on 2) The cascade distiller of claim 2 wherein the transportation channels comprise a wastewater fluid feed line, a wastewater fluid circulation loop, a condensation circulation loop, a processed fluid concentration loop, a distillate product effluent line, a vacuum line, an inter-cascade distribution line or any combination thereof. ### Claim 4 (depends on 1) The cascade distiller of claim 1 wherein the number of shaft sections is equal to the number of stages and wherein the number of stages is determined by the equation n opt = T max - T min Δ ⁢ ⁢ T 1 + Δ ⁢ ⁢ T d where nopt is the optimal number of cascades, Tmax and Tmin are the maximum and minimum possible temperatures, respectively, ΔTd is the temperature depression in a stage or cascade, ΔT1 is the temperature drop in one cascade, which is further defined by T1=Gdr/kFs where Gd is the amount of distillate produced in one cascade, r is the heat of vaporization of a liquid, k the heat transfer coefficient in a cascade and Fs the heat exchange surface of a cascade. ### Claim 5 (depends on 1) The cascade distiller of claim 1 wherein the number of stages is from about 2 to about 15. ### Claim 6 (depends on 1) The cascade distiller of claim 1 wherein assembly of the shaft sections to form the stationary shaft forms hydraulic seals between the stages. ### Claim 7 (depends on 1) The cascade distiller of claim 1 further comprising a plurality of Pitot pumps, the plurality of Pitot pumps being disposed uniformly on the periphery of the cylindrical rotor cover. ### Claim 8 (depends on 7) The cascade distiller of claim 7 wherein the plurality of Pitot pumps comprises: a feed Pitot pump in each stage of the cascade distiller; a pump Pitot pump in each stage of the cascade distiller, wherein the pump Pitot pump is located at a greater radial distance from the axis of rotation of the cylindrical rotor cover than the feed Pitot pump; and wherein the feed Pitot pump and the pump Pitot pump control fluid levels in each stage. ### Claim 9 (depends on 8) The cascade distiller of claim 8 wherein the feed Pitot pump of the first stage is controlled by an external valve wherein the external valve is open when the first feed Pitot pump experiences low Pitotostatic pressure in the first stage and closed when the feed Pitot pump experiences high Pitotostatic pressure in the first stage. ### Claim 10 (depends on 1) The cascade distiller of claim 1 wherein each shaft section comprises a part of a rotor body element, heat exchange surfaces, a partition, and a separator assembly. ### Claim 11 (depends on 1) The cascade distiller of claim 1 wherein each stage further comprises: the first opening and the second opening are disposed by the axis of rotation of the cylindrical rotor cover; and a vacuum line, the vacuum line being in communication between a vacuum pump and the cascade distiller and where non-condensing gases are removed from the cascade distiller through the first opening, second opening and the vacuum line. ### Claim 12 (depends on 1) The cascade distiller of claim 1 further comprising: at least one hydraulic seal between two adjoining stages, wherein the hydraulic seal comprises a fluid. ### Claim 13 (depends on 12) The cascade distiller of claim 12 wherein the hydraulic seal comprises a depth, wherein the depth is determined from the equation h ≥ Δ ⁢ ⁢ P ρ ⁢ ⁢ ω 2 ⁢ R where h is the depth of the hydraulic seal, ΔP is the pressure drop between cascades, ρ is the density of the fluid, ω is the angular velocity of rotation of the cylindrical rotor cover and R is the distance from the axis of rotation of said cylindrical rotor cover up to a nearest ridge of the hydraulic seal. ### Claim 14 (depends on 13) The cascade distiller of claim 13 wherein the hydraulic seal further comprises a width, wherein the width is determined by the equation δ ≤ 2 ⁢ σ 5 ⁢ ρ ⁢ ⁢ g ⁢ ⁢ h where δ is the width, σ is the surface tension of the liquid, g is gravity and h is the depth of the hydraulic seal. ### Claim 15 (depends on 12) The cascade distiller of claim 12 wherein the cascade distiller comprises two hydraulic seals, wherein one hydraulic seal located on an evaporation zone and the other hydraulic seal is located on a condensation zone. ### Claim 16 (depends on 12) The cascade distiller of claim 12 wherein the cascade distiller is operated under vacuum, microgravity, atmospheric pressure or overpressure. ### Claim 17 (depends on 12) The cascade distiller of claim 12 wherein the cascade stages are arranged sequentially within the cylindrical rotor cover and wherein a first cascade stage has the highest pressure and a last cascade stage has the lowest pressure. ### Claim 18 (depends on 12) The cascade distiller of claim 12 wherein the cascade stages further comprise a separator assembly, wherein the separator assembly is located by the center of the cylindrical rotor cover. ### Claim 19 (depends on 18) The cascade distiller of claim 18 wherein the separator assembly comprises at least two liquid traps and a separator fin assembly comprising radial fins and wherein the separator fin assembly comprises a convoluted path. ### Claim 20 (depends on 19) The cascade distiller of claim 19 wherein the fluid is condensate. ### Claim 21 (depends on 1) The cascade distiller of claim 1 further comprising: a first cascade stage and a last cascade stage, wherein neighboring cascade stages are in fluid communication; and a product condensation chamber, the product condensation chamber being in fluid communication with the last cascade stage, wherein the product condensation chamber comprises a first Pitot pump for pumping a condensate from the product condensation chamber to a condensation circulation loop and a second Pitot pump for pumping excess condensate to a distillate product effluent line. ### Claim 22 (depends on 21) The cascade distiller of claim 21 wherein the first Pitot pump is disposed near an outer wall of the cylindrical rotor cover and at a shallow depth. ### Claim 23 (depends on 21) The cascade distiller of claim 21 wherein the second Pitot pump has a smaller radius than the first Pitot pump and wherein the second Pitot pump is disposed at a maximum depth for the condensate in the product condensation chamber. ### Claim 24 (depends on 21) The cascade distiller of claim 21 wherein the condensation circulation loop is in fluid communication with a cooling side of a heat pump. ### Claim 25 (depends on 21) The cascade distiller of claim 21 wherein the radius of the second Pitot pump is from about 90% to about 98% of the radius of the first Pitot pump.