# US 7,608,164 B2 · Fabric-crepe process with prolonged production cycle and improved drying > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 7,608,164 B2 - Document ID: US7608164B2 - Status: Granted - Kind: B2 - Application number: 12/033,207 - Filed: 2008-02-19 - Published: 2008-10-30 - Granted: 2009-10-27 - Earliest claimed: 2007-02-27 - Assignees: Georgia-Pacific Consumer Products LP - Inventors: Hung Liang Chou; Mark S. Hunter; Kang Chang Yeh - Web page: https://patentgrep.com/patent/US7608164B2 ## CPC - D21F 11/14: Making cellulose wadding, filter or blotting paper - D21F 11/006: {Making patterned paper} - D21F: PAPER-MAKING MACHINES; METHODS OF PRODUCING PAPER THEREON ## Abstract A method of manufacturing absorbent sheet is directed to a wet-press/fabric-crepe process wherein add-on of adhesive to the Yankee surface is at relatively low levels, yet sheet transfer is maintained and production increased. Materials are selected and process parameters are controlled such that a paper machine can be operated for at least 4 hours before the Yankee coating needs to be stripped. Preferably, average increase in Yankee hood temperature is less than 1° F./minute during a production interval. ## Claims ### Claim 1 A method of making a fabric-creped absorbent cellulosic sheet comprising: (a) compactively dewatering a papermaking furnish to form a cellulosic web and concurrently applying the web to a heated rotating backing cylinder; (b) fabric-creping the web from the heated backing cylinder surface at a consistency of from about 30% to about 60% utilizing a patterned creping fabric, the creping step occurring under pressure in a fabric-creping nip defined between the backing cylinder surface and the creping fabric wherein the fabric is traveling at a second speed slower than the speed of said backing cylinder surface, the fabric pattern, nip parameters, velocity delta and web consistency being selected such that the web is creped from the backing cylinder surface and transferred into the creping fabric; (c) providing a hygroscopic, re-wettable resinous adhesive coating composition comprising a polyvinyl alcohol to a surface of a heated drying cylinder of a Yankee dryer at an add-on rate of less than 20 mg/m2 of drying cylinder surface such that a resinous adhesive coating is formed, the Yankee dryer also having a dryer hood with a characteristic operating temperature limit; (d) transferring the web from the creping fabric to the surface of the heated drying cylinder of the Yankee dryer such that the web is adhered to the drying cylinder by the resinous adhesive coating; (e) drying the web on the surface of the drying cylinder; (f) removing the dried web from the drying cylinder surface; and (g) periodically stripping at least a portion of the resinous adhesive coating from the drying cylinder surface as the characteristic operating temperature limit of the drying hood of the Yankee dryer is approached; wherein the furnish and resinous adhesive coating composition are selected and heating of the backing cylinder and drying cylinder is controlled such that a production interval between successive strippings of adhesive coating from the drying cylinder has a duration of at least 4 hours, and during which production interval a predetermined target production rate of dried sheet is met. ### Claim 2 (depends on 1) The method according to claim 1, wherein the add-on rate of resinous adhesive coating composition to the drying cylinder is less than 15 mg/m2 of drying cylinder surface. ### Claim 3 (depends on 1) The method according to claim 1, wherein the add-on rate of resinous adhesive coating composition to the drying cylinder is less than 10 mg/m2 of drying cylinder surface. ### Claim 4 (depends on 1) The method according to claim 1, wherein the add-on rate of resinous adhesive coating composition to the drying cylinder is from about 5 mg/m2 of drying cylinder surface to about 15 mg/m2 of drying cylinder surface. ### Claim 5 (depends on 1) The method according to claim 1, wherein the production interval between successive strippings of adhesive coating from the drying cylinder is from about 5 hours to about 15 hours. ### Claim 6 (depends on 1) The method according to claim 1, wherein the production interval between successive strippings of adhesive coating from the drying cylinder is at least about 5 hours. ### Claim 7 (depends on 1) The method according to claim 1, wherein the production interval between successive strippings of adhesive coating from the drying cylinder is at least about 7 hours. ### Claim 8 (depends on 1) The method according to claim 1, wherein the production interval between successive strippings of adhesive coating from the drying cylinder is at least about 10 hours. ### Claim 9 (depends on 1) The method according to claim 1, wherein the characteristic operating drying temperature limit of the drying hood is about 850° F. or less. ### Claim 10 (depends on 1) The method according to claim 1, wherein the drying hood is operated at an average air jet inlet temperature of from about 600° F. to about 850° F. during the production interval. ### Claim 11 (depends on 1) The method according to claim 1, wherein the resinous adhesive coating composition is durable up to a temperature of at least 240° F. ### Claim 12 (depends on 1) The method according to claim 1, wherein the resinous adhesive coating composition is durable up to a temperature of at least 300° F. ### Claim 13 (depends on 1) The method according to claim 1, wherein the dried sheet is removed from the drying cylinder at a sheet temperature of from about 240° F. to about 300° F. ### Claim 14 (depends on 1) The method according to claim 1, wherein the web is dried to a consistency of at least 90% prior to removal from the drying cylinder. ### Claim 15 (depends on 1) The method according to claim 1, wherein the web is dried to a consistency of at least 92.5% prior to removal from the drying cylinder. ### Claim 16 (depends on 1) The method according to claim 1, wherein the dried web is peeled from the drying cylinder surface. ### Claim 17 (depends on 1) The method according to claim 1, wherein the dried web is creped from the drying cylinder surface at a Reel Crepe of from about 2.5% to about 20%. ### Claim 18 (depends on 1) The method according to claim 1, wherein the web is transferred to the backing cylinder in a shoe press utilizing a pressure of more than 650 PLI. ### Claim 19 (depends on 1) The method according to claim 1, wherein the web is transferred to the backing cylinder in a shoe press utilizing a pressure of more than 700 PLI. ### Claim 20 (depends on 1) The method according to claim 1, wherein the web is transferred to the backing cylinder in a shoe press utilizing a pressure of from about 675 PLI to about 775 PLI. ### Claim 21 (depends on 1) The method according to claim 1, wherein the backing roll is heated with steam at a pressure of more than 60 psig. ### Claim 22 (depends on 1) The method according to claim 1, wherein the backing roll is heated with steam at a pressure of more than 75 psig. ### Claim 23 (depends on 1) The method according to claim 1, wherein the backing roll is heated with steam at a pressure of more than 90 psig. ### Claim 24 (depends on 1) The method according to claim 1, wherein the backing roll is heated with steam at a pressure of from about 80 psig to about 150 psig. ### Claim 25 (depends on 1) The method according to claim 1, wherein the Yankee drying cylinder is heated with steam at a pressure of from about 90 psig to about 110 psig. ### Claim 26 (depends on 1) The method according to claim 1, wherein dried sheet production is substantially constant during a production interval between successive strippings of adhesive coating form the drying cylinder. ### Claim 27 (depends on 1) The method according to claim 1, wherein the target production of dried sheet is at least 2000 fpm. ### Claim 28 (depends on 1) The method according to claim 1, wherein the target production of dried sheet is at least 2250 fpm. ### Claim 29 (depends on 1) The method according to claim 1, wherein the target production of dried sheet is at least 2500 fpm. ### Claim 30 A method of making a fabric-creped absorbent cellulosic sheet comprising: (a) compactively dewatering a papermaking furnish to form a web and concurrently applying the web to a heated rotating backing cylinder; (b) fabric-creping the web from the backing cylinder surface at a consistency of from about 30% to about 60% utilizing a patterned creping fabric, the creping step occurring under pressure in a fabric-creping nip defined between the backing cylinder surface and the creping fabric wherein the fabric is traveling at a second speed slower than the speed of said backing cylinder surface, the fabric pattern, nip parameters, velocity delta and web consistency being selected such that the web is creped from the backing cylinder surface and transferred into the creping fabric; (c) providing a hygroscopic, re-wettable resinous adhesive coating composition comprising a polyvinyl alcohol to a surface of a heated drying cylinder of a Yankee dryer at an add-on rate of about 15 mg/m2 of drying cylinder surface or less such that a resinous adhesive coating is formed, the Yankee dryer also having a dryer hood configured to provide drying energy to the web on the Yankee drying cylinder in the form of a heated air stream, the hood having a characteristic operating temperature and a characteristic operating temperature limit; (d) transferring the web from the creping fabric to the surface of the heated drying cylinder of the Yankee dryer such that the web is adhered to the drying cylinder by the resinous adhesive coating; (e) drying the web to a predetermined dryness on the surface of the drying cylinder; (f) removing the dried web from the drying cylinder surface; and (g) periodically stripping at least a portion of the resinous adhesive coating from the drying cylinder surface as the characteristic operating temperature limit of the drying hood of the Yankee dryer is approached; wherein the furnish and resinous adhesive coating composition are selected and heating of the backing cylinder and drying cylinder is controlled and such that a production interval between successive strippings of adhesive coating from the drying cylinder has a duration of at least 4 hours, and during which production interval a predetermined target production rate of dried sheet is met, the production interval further characterized in that the average rate of increase of the characteristic operating temperature of the dryer hood over the production interval is less than 1° F./minute. ### Claim 31 (depends on 30) The method according to claim 30, wherein the average rate of increase of the characteristic operating temperature of the dryer hood over the production interval is less than 0.75° F./min. ### Claim 32 (depends on 30) The method according to claim 30, wherein the average rate of increase of the characteristic operating temperature of the dryer hood over the production interval is less than 0.5° F./min. ### Claim 33 (depends on 30) The method according to claim 30, wherein the dryer hood is provided drying energy at a rate of less than 3 MMBtu/ton for a duration of at least 30 minutes during the production interval. ### Claim 34 (depends on 30) The method according to claim 30, wherein the dryer hood is provided drying energy at a rate of less than 3 MMBtu/ton for a duration of at least 60 minutes during the production interval. ### Claim 35 (depends on 30) The method according to claim 30, wherein the resinous adhesive coating composition provided to the drying cylinder includes a polyvinyl alcohol resin and a polyamidoamine resin. ### Claim 36 (depends on 35) The method according to claim 35, wherein the resinous adhesive coating composition provided to the drying cylinder includes less than 75% by weight of polyvinyl alcohol resin. ### Claim 37 (depends on 35) The method according to claim 35, wherein the resinous adhesive coating composition provided to the drying cylinder includes less than 65% by weight of polyvinyl alcohol resin. ### Claim 38 (depends on 35) The method according to claim 35, wherein the resinous adhesive coating composition provided to the drying cylinder includes less than 60% by weight of polyvinyl alcohol resin. ### Claim 39 (depends on 35) The method according to claim 35, wherein the resinous adhesive coating composition provided to the drying cylinder includes less than 50% by weight of polyvinyl alcohol resin. ### Claim 40 (depends on 35) The method according to claim 35, wherein the resinous adhesive coating composition provided to the drying cylinder includes from about 40% by weight to about 80% by weight of polyvinyl alcohol resin. ### Claim 41 (depends on 35) The method according to claim 35, wherein the resinous adhesive coating composition provided to the drying cylinder includes from about 5% by weight polyamidoamine resin to about 35% by weight polyamidoamine resin. ### Claim 42 (depends on 35) The method according to claim 35, wherein the resinous adhesive coating composition provided to the drying cylinder includes at least 10% by weight of a polyamidoamine resin. ### Claim 43 (depends on 35) The method according to claim 35, wherein the resinous adhesive coating composition includes from about 2.5 weight % modifier to about 30 weight % modifier. ### Claim 44 (depends on 35) The method according to claim 35, wherein the resinous adhesive coating composition contains up to about 20 weight % modifier. ### Claim 45 (depends on 35) The method according to claim 35, wherein the resinous adhesive coating composition contains up to about 30 weight % modifier. ### Claim 46 A method of making a fabric-creped absorbent cellulosic sheet comprising: (a) preparing an aqueous papermaking furnish including pulp comprising pre-dried papermaking fibers which have been dried to at least 80% air-dry prior to preparing the aqueous furnish; (b) depositing the papermaking furnish on a formaninous support; (c) compactively dewatering the papermaking furnish to form a nascent web and concurrently applying the web to a heated rotating backing cylinder; (d) fabric-creping the web from the heated backing cylinder surface at a consistency of from about 30% to about 60% utilizing a patterned creping fabric, the creping step occurring under pressure in a fabric-creping nip defined between the backing cylinder surface and the creping fabric wherein the fabric is traveling at a second speed slower than the speed of said backing cylinder surface, the fabric pattern, nip parameters, velocity delta and web consistency being selected such that the web is creped from the backing cylinder surface and transferred into the creping fabric; (e) providing a hygroscopic, re-wettable resinous adhesive coating composition comprising a polyvinyl alcohol to a surface of a heated drying cylinder of a Yankee dryer at an add-on rate of about 15 mg/m2 of drying cylinder surface or less such that a resinous adhesive coating is formed, the Yankee dryer also having a drying hood with a characteristic operating temperature limit; (f) transferring the web from the creping fabric to the surface of the heated drying cylinder of the Yankee dryer such that the web is adhered to the drying cylinder by the resinous adhesive coating; (g) drying the web to a predetermined dryness on the surface of the drying cylinder; (h) removing the dried web from the drying cylinder surface; and (i) periodically stripping at least a portion of the resinous adhesive coating from the drying cylinder surface as the characteristic operating temperature limit of the drying hood of the Yankee dryer is approached; wherein the furnish and resinous adhesive coating composition are selected and heating of the backing cylinder and drying cylinder is controlled such that a production interval between successive strippings of adhesive coating from the drying cylinder has a duration of at least 4 hours, and during which production interval a target production rate of dried sheet is met. ### Claim 47 (depends on 46) The method according to claim 46, wherein the pre-dried papermaking fibers are dried to at least 90% air-dry prior to preparing the aqueous papermaking furnish. ### Claim 48 (depends on 46) The method according to claim 46, wherein the pre-dried papermaking fibers are dried to at least 95% air-dry prior to preparing the aqueous papermaking furnish. ### Claim 49 (depends on 46) The method according to claim 46, wherein the pre-dried papermaking fibers include Southern Softwood Kraft fiber. ### Claim 50 (depends on 46) The method according to claim 46, wherein the pre-dried fiber has a GE brightness of at least 80. ### Claim 51 (depends on 46) The method according to claim 46, wherein the pre-dried fiber has a GE brightness of at least 85. ### Claim 52 (depends on 46) The method according to claim 46, wherein the pre-dried fiber has a GE brightness of at least 90. ### Claim 53 (depends on 46) The method according to claim 46, wherein the pre-dried papermaking fibers have a GE brightness of between about 85 and 95. ### Claim 54 (depends on 46) The method according to claim 46, wherein the pulp in the furnish comprises at least 60% by weight pre-dried fiber. ### Claim 55 (depends on 46) The method according to claim 46, wherein the pulp in the furnish comprises at least 75% by weight pre-dried fiber.