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US 7,598,405 B2Granted
Method for the distillative processing of tetrahydrofuran
AssigneeBASF SE
InventorsGunther Windecker, Alexander Weck, Markus Roesch, Michael Steiniger, Rolf Pinkos, Dany Vanden Hautte
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Abstract
The present invention provides a process for distillatively purifying tetrahydrofuran in the presence of a polar solvent.
Claims11
A process for reducing a butyl methyl ether content of tetrahydrofuran comprising:
- adding methanol to a tetrahydrofuran feed stream comprising butyl methyl ether to form a THF mixture;
- distilling the THF mixture in one or more distillation stages in a single separating apparatus;
- removing a top draw from an upper portion of the separating apparatus;
- and
- removing bottom draw from a lower portion of the separating apparatus;
- wherein
- a content of butyl methyl ether in % by weight in the top draw is greater than the content of butyl methyl ether in the THF mixture, and
- a content of butyl methyl ether in % by weight in the bottom draw is less than the butyl methyl ether content in the tetrahydrofuran feed stream.
5 more elements
Dependencies are inferred from the claim text.