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US 7,351,765 B2Granted
Method for producing polyvinylacetals
AssigneeWacker Polymer Systems GmbH & Co. KG
InventorsKurt Stark, Peter Tschirner, Karl-Heinz Eichel, Georg Friedl, Franz Eichberger
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Abstract
Polyvinyl acetals are obtained in a cost-effective and environmentally advantageous manner by employing as at least a portion of the aqueous acetalization medium, the mother liquor from a previous acetalization reaction.
Claims10
A process for preparing polyvinyl acetals by hydrolysis of a vinyl ester polymer and acetalization of the resultant polyvinyl alcohol with one or more aldehydes selected from the group consisting of aliphatic and aromatic aldehydes having 1 to 15 carbon atoms, comprising:
- a) providing a polyvinyl alcohol to form an initial charge in an aqueous medium,
- b) if necessary, adding acid to adjust to a pH of <1,
- c) initiating acetalization by addition of an aldehyde component, and
- d) precipitating polyvinyl acetal and separating polyvinyl acetal via filtration from a filtrate,
- wherein from 10 to 100% by weight of the aqueous medium of a) comprises the filtrate from a preceding batch of polyvinyl acetal production, and, optionally reusing the filtrate produced in d) in a further polyvinyl acetal production batch.
2 more elements
Dependencies are inferred from the claim text.