Spectroscopy-based real-time control for microwave-assisted chemistry

Abstract

The invention is an instrument and method for microwave-assisted chemical synthesis. The instrument includes a source of microwave radiation for applying microwave energy to a sample, a microwave cavity in wave communication with the source for holding the sample during the application of microwave energy, and a substantially monochromatic radiation source in electromagnetic communication with the cavity for applying substantially monochromatic light to the sample. The instrument further includes a detector positioned to detect Raman scattering of light from the monochromatic source by the sample, and a controller in signal communication with the microwave energy source and the Raman scattering detector for moderating the application of microwave energy to the sample based upon the detected Raman scattering.

Dependencies are inferred from the claim text.