# US 7,073,562 B2 · Method for producing a monocrystalline component, having a complex moulded structure > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 7,073,562 B2 - Document ID: US7073562B2 - Status: Granted - Kind: B2 - Application number: 10/486,606 - Filed: 2002-07-24 - Published: 2005-06-09 - Granted: 2006-07-11 - Earliest claimed: 2001-08-13 - Assignees: Siemens Aktiengesellschaft - Applicants: Iris Oltmanns, legal representative - Web page: https://patentgrep.com/patent/US7073562B2 ## CPC - C30B 11/003: {Heating or cooling of the melt or the crystallised material} - C30B 11/00: Single-crystal growth by normal freezing or freezing under temperature gradient, e.g. Bridgman-Stockbarger method (C30B13/00, C30B15/00, C30B17/00, C30B19/00 take precedence; under a protective fluid C30B27/00) - C30B 29/52: Alloys - C30B: SINGLE-CRYSTAL GROWTH (by using ultra-high pressure, e.g. for the formation of diamonds, B01J3/06); UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL (zone-refining of metals or alloys C22B); PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE (casting of metals, casting of other substances by the same processes or devices B22D; working of plastics B29; modifying the physical structure of metals or alloys C21D, C22F); SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE (for producing semiconductor devices or parts thereof H10); APPARATUS THEREFOR ## Abstract The invention relates to a method for producing a monocrystalline component, having a complex moulded structure with different structure parts, from a molten metal. According to the method, said molten metal is located in a negative mould, corresponding to the moulding structure and said negative mould moves with the formation of a solidification front on a temperature drop, which is adapted to the crystallization speed of the molten metal and which includes the melting point. Said method is characterized in that at least one of the structure parts of the moulded structure experiences an individual temperature drop. If the solidification front has to grow through a structure part, which is inappropriately oriented in relation to the solidification front, said structure part or zone can experience an individual temperature drop. This enables monocrystalline components, having a complex moulded structure, to be produced in a reliable and economic manner. ## Claims ### Claim 1 A process for producing a single-crystal structural component with a complex shape, comprising: melting a metal; introducing the metal melt into a mold which correlates with the shape of the component; moving the mold through a temperature gradient matched to the crystallization rate of the metal melt and including the melting point; and forming a solidification front on the metal melt, wherein an individual temperature gradient is generated for a plurality of structural portions of the component, wherein the individual temperature gradient is formed by an independently actuable heating element. ### Claim 2 (depends on 1) The process as claimed in claim 1, wherein a plurality of temperature gradients form a plurality of solidification fronts. ### Claim 3 (depends on 1) The process as claimed in claim 1, wherein different individual temperature gradients are advanced at different speeds. ### Claim 4 (depends on 1) The process as claimed in claim 1, wherein individual temperature gradients of different portions of the components have individual orientations with respect to a crystal growth direction of the metal melt. ### Claim 5 (depends on 4) The process as claimed in claim 4, wherein the different crystal growth directions of the different structural parts substantially follow a main crystal growth direction. ### Claim 6 (depends on 4) The process as claimed in claim 4, wherein the different crystal growth directions deviate by no more than 20° from the main crystal growth direction. ### Claim 7 (depends on 1) The process as claimed in claim 1, wherein an induction coil and/or a radiator is used as the heating element. ### Claim 8 (depends on 7) The process as claimed in claim 7, wherein the temperature gradient is influenced by an insulation body. ### Claim 9 (depends on 1) The process as claimed in claim 1, wherein the component is a turbine vane. ### Claim 10 (depends on 1) The process as claimed in claim 1, wherein the temperature gradient is a negative temperature gradient. ### Claim 11 A process for producing a single-crystal structural component with a complex shape, the process comprising: introducing a metal melt into a mold which correlates with the shape of a component and comprises a first region extending in a first direction along a longitudinal axis and a second region extending at an angle inclined with respect to the longitudinal axis; and introducing into the metal melt a first negative temperature gradient to form a first solidification front moving through the first region in the first direction and a second negative temperature gradient to form a second solidification front moving through the second region in the second direction effective to form the component in a single crystal growth, wherein the component is a turbine blade, and further comprising the first negative temperature gradient causing the first solidification front to progress along a longitudinal axis of an airfoil portion of the blade and the second negative temperature gradient causing the first solidification front to bend into a platform section of the blade to form the second solidification front that progresses through the platform substantially perpendicular to the longitudinal axis. ### Claim 12 (depends on 11) The process of claim 11, wherein one of the solidification fronts is a planar solidification front and another of the solidification fronts is a shaped solidification front. ### Claim 13 (depends on 11) The process of claim 11, wherein the first and second solidification fronts advance at different speeds.