# US 6,773,483 B2 · Sodium purification method

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- Number: US 6,773,483 B2
- Document ID: US6773483B2
- Status: Granted
- Kind: B2
- Application number: 10/146,067
- Filed: 2002-05-16
- Published: 2002-11-21
- Granted: 2004-08-10
- Earliest claimed: 2001-05-16
- Assignees: Mssa
- Inventors: Pierre Flacher
- Web page: https://patentgrep.com/patent/US6773483B2

## CPC

- C22B 26/10: Obtaining alkali metals
- C22B 9/05: Refining by treating with gases, e.g. gas flushing {also refining by means of a material generating gas in situ}
- C22B: PRODUCTION AND REFINING OF METALS (electrolytic C25); PRETREATMENT OF RAW MATERIALS

## Abstract

The invention relates to a technical sodium purification method consisting of placing liquid sodium in contact at a temperature greater than or equal to 150° C., inside a static mixer, with an inert gas stream with respect to the sodium containing the stoechiometric quantity of water vapour required to oxidise calcium so as to lower its content to the desired content, and then separating the purified sodium from the inert gas, and the hydrogen and lime produced by the reaction.

## Claims

### Claim 1

A continuous sodium purification method for reducing the calcium content of sodium, comprising:
placing unpurified liquid sodium in contact with a stream of a gas, at a temperature of at least 150° C., wherein the stream of the gas comprises water vapor and the gas is inert with respect to unpurified liquid sodium;
adding water to the gas in a stoichiometric quantity sufficient to oxidize calcium so as to lower the content of calcium in the unpurified liquid sodium to a desired level and thereby produce purified sodium comprising the gas, hydrogen and lime;
regulating a flow rate of the water according to a flow rate of the liquid sodium so as to create and/or maintain a substantially constant ratio of the flow rate of the water to the flow rate of the liquid sodium; and
separating the purified sodium from the gas, the hydrogen and the lime.

### Claim 2 (depends on 1)

A method according to claim 1, wherein the inert gas comprises nitrogen or argon.

### Claim 3 (depends on 1)

A method according to claim 1, wherein the purified sodium is filtered to separate the lime.

### Claim 4 (depends on 1)

A method according to claim 1, wherein the gas comprises nitrogen, and wherein the nitrogen is present in an amount of 30 to 40 dm3 per gram of water contained in the stream of the gas.

### Claim 5 (depends on 1)

A method according to claim 1, further comprising placing the liquid sodium and the gas in contact in a static mixer.