A process for regenerating an at least partly reduced catalytic redox solution comprising at least one polyvalent metal chelated by a chelating agent and being circulated in at least one regeneration zone while injecting an oxygen-containing gas into the regeneration zone, the process comprising:
- measuring a concentration of oxygen dissolved in a regeneration zone effluent and adjusting a flow rate of the at least partly reduced catalytic redox solution entering the at least one regeneration zone and/or an oxygen-containing gas entering the regeneration zone in response to a measured concentration of oxygen, until a concentration of oxygen in the regeneration zone effluent is less than 20% of an amount of oxygen dissolved in water saturated with oxygen, thereby minimizing degradation of the chelating agent in the catalytic redox solution.