Method for preparing (meth) acrylic acid ester
AssigneeNippon Shokubai Co., Ltd.
InventorsSei Nakahara, Masatoshi Ueoka
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AssigneeNippon Shokubai Co., Ltd.
InventorsSei Nakahara, Masatoshi Ueoka
Estimating the term…
An improvement is provided in a method for preparing an (meth)acrylic acid ester comprising an esterification step for forming the (meth)acrylic acid ester by esterification reaction between (meth)acrylic acid and the corresponding aliphatic alcohol having 1 to 4 carbon atoms in the presence of an acidic catalyst, and a separation-purification step comprising an acid-separating column, a low boiling matter-separating column and a rectification column for separating and purifying the (meth)acrylic acid ester from the (meth)acrylic acid ester-containing mixture obtained in the esterification step. This improvement lies in that by circulating the bottom residue of the rectification column into the esterification step and/or the separation-purification step, the remaining polymerization inhibitor in the bottom residue is effectively reused and the remaining (meth)acrylic acid ester in the bottom residue is efficiently recovered.
A method for preparing an (meth)acrylic acid ester comprising
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