Process for producing laurolactam from cyclododecanone
AssigneeUbe Industries, Ltd.
InventorsNobuyuki Kuroda, Joji Kawai, Hideo Shimomura
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Abstract
Laurolactam having high quality is produced by reacting cyclododecanone with a hydroxylamine salt of a mineral acid, and converting the resultant cyclododecanoneoxime to laurolactam through the Beckmann rearrangement reaction, wherein a content of each of oxygen atom-containing C12 organic compounds, for example, cyclododecenone or epoxycyclododecane, and cycloaliphatic unsaturated C12 hydrocarbon compounds, contained, as an impurity, in the staring cyclododecanone material, is controlled to 1,000 ppm or less.
Claims9
A process for producing laurolactam from cyclododecanone, comprising reacting cyclododecanone with a hydroxylamine salt of a mineral acid to prepare cyclododecanoneoxime, and converting the resultant cyclododecanoneoxime to laurolactam through the Beckmann rearrangement reaction,
- wherein a content of each of the oxygen atom-containing organic compounds having 12 carbon atoms and cycloaliphatic unsaturated hydrocarbon compounds having 12 carbon atoms, contained, as an impurity, in the cyclododecanone used as a starting material, is controlled to 1,000 ppm or less.
Dependencies are inferred from the claim text.