Sol-gel derived sorbents
AssigneeUT-Battelle, LLC
InventorsMichael E. Sigman, Amy B. Dindal
Life of this patent
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AssigneeUT-Battelle, LLC
InventorsMichael E. Sigman, Amy B. Dindal
Estimating the term…
Described is a method for producing copolymerized sol-gel derived sorbent particles for the production of copolymerized sol-gel derived sorbent material. The method for producing copolymerized sol-gel derived sorbent particles comprises adding a basic solution to an aqueous metal alkoxide mixture for a pH≦8 to hydrolyze the metal alkoxides. Then, allowing the mixture to react at room temperature for a precalculated period of time for the mixture to undergo an increased in viscosity to obtain a desired pore size and surface area. The copolymerized mixture is then added to an immiscible, nonpolar solvent that has been heated to a sufficient temperature wherein the copolymerized mixture forms a solid upon the addition. The solid is recovered from the mixture, and is ready for use in an active sampling trap or activated for use in a passive sampling trap.
A method for producing copolymerized sol-gel derived sorbent particles comprising the steps of:
Dependencies are inferred from the claim text.