Method of making microporous structure defined by a multiplicity of singular channels
AssigneeUop LLC
InventorRoy V. Semerdjian
Life of this patent
Estimating the term…
Abstract
A microporous structure can be formed from ductile material such as glass into an axially extended outer wall surrounding a plurality of singular micro-passages surrounded by the outer wall to provide an open area that extends continuously over the length of the outer wall. The diameter of the micro-passages will usually not exceed 25 μm and are more in range of from 0.5 to 5 μm. The structure is particularly useful as frits for the containment of packing in capillaries for chromatograph applications and more generally as flow restrictors. Continuous open diameters of the micro-passages have a relatively straight flow path that reduces pressure drop relative to the random arrangement of other frits while still providing the desired containment.
Claims8
A method of forming a microporous structure comprising an axially extended outer wall that surrounds a plurality of singular micro-passages defined by internal walls and wherein the micro-passages extend along the axial length of the outer wall, the method comprising:
- a) inserting a plurality of conduits into a surrounding tube to form a tube and conduit assembly wherein the conduits have relatively small internal and external diameters relative to the tube;
- b) sealing the common openings of the conduits about one end of the tube and conduit assembly to form a drawing preform having a closed end about which all conduits are sealed from fluid flow and an opposite open end about which all conduits are open for fluid flow;
- c) heating the drawing preform to a softening temperature that permits plastic flow of the drawing stock under an axial traction force but inhibits plastic flow of the drawing stock under its own weight;
- d) simultaneously drawing the drawing preform by application of a tractor while maintaining the preform at the softening temperature and restricting fluid flow from the open end to reduce the interiors of the conduits to a micropore size while preventing collapsing closure of the conduit interiors;
- and,
- e) collecting a microporous structure from the drawn drawing stock that has a plurality of singular micro-passages defined by internal walls and substantially equal in number to the number of conduits.
Dependencies are inferred from the claim text.