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US 6,637,239 B2Granted
Nitrogen rejection method and apparatus
AssigneeThe BOC Group, Inc.
InventorJohn Douglas Oakey
Life of this patent
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AssigneeThe BOC Group, Inc.
InventorJohn Douglas Oakey
Estimating the term…
Nitrogen is rejected from a feed gas stream comprising methane and nitrogen so as to form a methane product. The feed gas stream is cooled in a main heat exchanger and is rectified in a double rectification column comprising a higher pressure rectification column, a lower pressure rectification column, and a condenser-reboiler placing the higher pressure rectification column in heat exchange relationship with the lower pressure rectification column. At least part of the feed gas stream is expanded into the higher pressure rectification column through an expansion valve, the feed gas stream being partially liquefied upstream of the double rectification column. Over a period of time the mole fraction of nitrogen in the feed gas mixture increases. At a suitable increased nitrogen mole fraction, operation of a second double rectification column in parallel with the first double rectification column is commenced.
A method of rejecting nitrogen from a feed gas stream comprising methane and nitrogen so as to form a methane product, the mole fraction of nitrogen in the feed gas increasing over a period of time, the method comprising cooling the feed gas stream in a main heat exchanger, rectifying the cooled feed gas stream in a first double rectification column comprising a higher pressure rectification column, a lower pressure rectification column, and a condenser-reboiler placing the higher pressure rectification column in heat exchange relationship with the lower pressure rectification column, expanding at least part of the feed gas stream into the higher pressure rectification column, partially liquefying the feed gas stream upstream of the first double rectification column, and operating a second double rectification column in parallel with the first double rectification column when the nitrogen mole fraction in the feed gas stream has a mole fraction value of 0.4.
Apparatus for rejecting nitrogen from a feed gas stream comprising methane and nitrogen so as to form a methane product, the apparatus comprising a main heat exchanger for cooling the feed gas stream, a double rectification column for rectifying the feed gas stream comprising a higher pressure rectification column, a lower pressure rectification column, a condenser-reboiler placing the higher pressure rectification column in heat exchange relationship with the lower pressure rectification column, and an expansion device downstream of the main heat exchanger communicating with the higher pressure rectification column, the expansion device being arranged for introducing a part of the feed gas stream into the higher pressure rectification column in liquid state, wherein there is a second double rectification column in parallel with the first double rectification column and there is a back pressure regulating valve associated with the lower pressure rectification column of the first double rectification column which back pressure regulating valve is operable to increase the pressure n said lower pressure rectification column.
Dependencies are inferred from the claim text.