US 6,591,663 B1Granted

Viscosity and viscoelasticity measuring instrument

AssigneeBoston Rheology, Inc.

InventorsPaul D. Murray, Alfredo O. Kenig, David Porat

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Abstract

A viscosity and viscoelasticity measuring instrument has a cam, a follower arm, a flat spring, a plate fixture, and a removable plate assembly. The cam is a rotating circular disk with a spiral slot. A cam follower on the follower arm resides in the spiral slot so that the follower arm pivots about its fixed end as the cam rotates. The spring is attached to and collinear with the fixed end of the follower arm so that the spring pivots in the opposite direction as the follower arm. The removable plate assembly has a lower plate and an upper plate with mating sample surfaces on which test fluid is placed. The lower plate fits into a lower jaw of the plate fixture that is attached to the instrument base. The upper plate fits into an upper jaw of the plate fixture attached to the free end of the spring. A fluid is placed on the lower sample surface. The cam rotates, pushing the follower arm up, causing the spring to pivot down, and pressing the sample surfaces together. The cam is reversed, causing the spring to impart a separation force to the plates. The time it takes for the plates to separate is measured and converted to a viscosity value.

An instrument for measuring the viscosity of a fluid sample, said instrument comprising:

(a) a housing having a base;
(b) a cam, said cam being a disk with a cam axis and a spiral slot about said axis;
(c) a rotation means for rotating said cam about said cam axis;
(d) a cam follower arm having a fixed end and a free end, said cam follower arm being pivotally mounted to said base at said cam follower arm fixed end, said cam follower arm having a cam follower residing in said cam spiral slot, such that, as said cam rotates, said cam follower arm pivots about said cam follower arm fixed end;
(e) a spring, said spring being a flat strip mounted to said cam follower arm fixed end approximately collinear with said cam follower arm, said spring having a free end remote from said cam follower arm;
(f) a plate fixture having a lower jaw and an opposing upper jaw, said lower jaw attached to said base and said upper jaw attached to said spring free end;
(g) a plate assembly comprising a lower plate and an upper plate, said lower plate having a lower sample surface, said upper plate having an upper sample surface, said plate assembly being removably installable in said plate fixture such that said lower plate seats in said lower jaw and said upper plate seats in said upper jaw;
and
(h) a controller for controlling the operation of said instrument;
(i) whereby said fluid sample is placed on said lower sample surface, said plate assembly is installed in said plate fixture, said cam rotates forwardly such that said cam follower arm pivots upwardly causing said spring free end to pivot downwardly to press said upper sample surface to said lower sample surface at a predetermined compression force for a predetermined amount of time, said cam rotating reversely such that said cam follower arm pivots downwardly causing said spring free end to pivot upwardly to apply a separation force between said upper sample surface and said lower sample surface until said sample fluid fractures, said controller measuring the amount of time from a predetermined time to when said fluid sample fractures as a separation time, said predetermined time being no later than when said cam begins to rotate reversely.

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Abstract

Claims11