Method for separating catalyst, product and solvent
AssigneesSumitomo Chemical Company, Limited, Daicel Chemical Industries, Ltd.
InventorsNobuhiro Tani, Shuzo Murata
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AssigneesSumitomo Chemical Company, Limited, Daicel Chemical Industries, Ltd.
InventorsNobuhiro Tani, Shuzo Murata
Estimating the term…
A method for separating an oxidation catalyst, an oxidation reaction product and a reaction solvent from a reaction mixture obtained by oxidizing a substrate in the presence of an oxidation catalyst containing an aromatic N-hydroxyimide compound and a transition metal, the method including (i) distilling the reaction solvent from the reaction mixture in the presence of an organic solvent which is immiscible with the reaction solvent to obtain the reaction mixture containing the reaction solvent in an amount of 5 parts by weight or less per one part by weight of the N-hydroxyimide compound, and the oxidation catalyst precipitated, and (ii) separating the reaction mixture obtained in the step (i) by a solid-liquid separation method into the oxidation product and the oxidation catalyst.
A method for separating an oxidation catalyst, a product of an oxidation reaction and a reaction solvent from a reaction mixture obtained by oxidizing a substrate in the presence of an oxidation catalyst which comprises an aromatic N-hydroxyimide compound and a transition metal, the method comprising the steps of:
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