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US 6,486,335 B1Granted
Process for the preparation of refined hard sugarcane wax having improved qualities from press mud
AssigneeCouncil of Scientific & Industrial Research (CSIR)
InventorAmal C. Phukan
Life of this patent
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Abstract
The present invention relates to a process for the preparation of refined hard sugarcane wax having improved qualities from press mud which comprises digesting press mud with a non polar solvent in the presence of activated charcoal and separating the sugarcane wax from the residue.
Claims3
A process for the preparation of refined hard sugarcane wax having improved qualities from press mud which comprises:
- (a) digesting press mud with a non polar solvent such as carbon tetrachloride (CCl4), benzene (C6H6) or toluene (C7HB) in presence of activated charcoal, wherein the ratio of the non polar solvent to activated charcoal:
- press mud ranges from 3 liters to 1.50 liters:50 gm to 20 gm:1 kg to 500 gm (60 to 75:1:20 to 25):
- (b) separating the residue by known methods;
- (c) removing the solvent by conventional methods followed by treating the crude sugarcane wax obtained with hot isopropyl alcohol to get the wax in solution and pitch as residue;
- (d) separating the said wax in solution by known methods and cooling to room temperature so as to get the said wax precipitated;
- (e) washing thoroughly with water till the isopropyl alcohol is removed and drying to get the hard sugarcane wax;
- (d) if desired recycling the isopropyl alcohol (I.P.A.) to step (c) and then treating the said sugarcane wax with hot water for further refining.
4 more elements
Dependencies are inferred from the claim text.