Method of preparing a mixture of mannitol and sorbitol by continuous hydrogenation of glucosone
AssigneeRoquette Freres
InventorsJean-Christophe Choque, Guy Fleche
Life of this patent
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Abstract
The invention relates to a method of preparing a mixture of mannitol and sorbitol, charactertized by the fact that continuous hydrogenation of glucosone with a solid matter content equal to at least 30%, preferably between 30 and 50%, is carried out in a succession of fixed catalyst beds disposed in series, which includes a first hydrogenation zone, made up of at least one fixed catalyst bed where hydrogenation is carried out at a temperature equal at the most to 80° C., preferably between 50 and 80° C., and a second hydrogenation zone, made up of at least one fixed catalyst bed where hydrogenation is carried out at a temperature equal to at least 80° C., preferably between 100 to 150° C.
Claims18
A method of preparing a mixture of mannitol and sorbitol, wherein continuous hydrogenation of glucosone with a solid matter equal to at least 10% is carried out in a succession of fixed catalyst beds disposed in series, which includes:
- a first hydrogenation zone, made up of at least one fixed catalyst bed, wherein hydrogenation is carried out at a temperature equal at the most to 80° C.;
- and
- a second hydrogenation zone, made up of at least one fixed catalyst bed, wherein the hydrogenation is carried out at a temperature equal to at least 80° C.
Dependencies are inferred from the claim text.