Process and installation for separation of air by cryogenic distillation
AssigneeL'Air Liquide, Societe Anonyme Aodirectoire et Conseil de Surveillance pour l'Etude et l'Exploitation des Procedes Georges Claude
InventorJean Renaud Brugerolle
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Abstract
In an apparatus for the separation of air by cryogenic distillation, the overhead gas of a mixing column is sent to the passages for warming a bottom reboiler of the low-pressure column of a double column fed with air to be distilled. The production of oxygen in the bottom of the low-pressure column is increased.
Claims32
Air separation plant for producing an oxygen-rich fluid by cryogenic distillation, comprising:
- a double column comprising at least one medium-pressure column and a low-pressure column which includes a reboiler for vaporizing liquid in the bottom of the low-pressure column;
- a mixing column;
- means for sending cooled and compressed air to at least the medium-pressure column;
- means for sending an oxygen-enriched liquid from the medium-pressure column to an injection point of the low-pressure column and a nitrogen-enriched liquid from the medium-pressure column to the low-pressure column;
- means for sending gas to the bottom of the mixing column;
- means for sending a second oxygen-enriched liquid from the low-pressure column to the top of the mixing column, the second liquid being less volatile than the gas feeding the bottom of the mixing column;
- means for withdrawing an oxygen-rich fluid from the low-pressure column;
- means for sending at least one portion of a gas from the mixing column to passages for warming the reboiler,
- wherein the means for sending the second liquid further comprises means for withdrawing the second liquid from the low-pressure column at a level at least 5 theoretical trays below the injection point of the low-pressure column.
Air separation plant for producing an oxygen-rich fluid and argon by cryogenic distillation, comprising:
- a double column comprising a medium-pressure column and a low-pressure column which includes a reboiler for vaporizing liquid in the bottom of the low-pressure column;
- an argon column comprising a condenser;
- a mixing column;
- means for sending cooled and compressed air to the medium-pressure column;
- means for sending a first oxygen-enriched liquid from the medium-pressure column to the condenser;
- means for withdrawing an argon-enriched gas from a first level of the low-pressure column and means for sending the argon-enriched gas to the argon column;
- means for sending an oxygen-enriched liquid and a nitrogen-enriched liquid from the medium-pressure column to the low-pressure column;
- means for at least partially vaporizing oxygen-enriched liquid in the condenser and means for sending at least one portion of the vapor and/or air to the bottom of the mixing column;
- means for sending a second oxygen-enriched liquid from the low-pressure column to the top of the mixing column, the second liquid being less volatile than the gas feeding the bottom of the mixing column;
- means for withdrawing an argon-enriched fluid at the top of the argon column;
- means for withdrawing an oxygen-rich fluid at the low-pressure column;
- and
- means for sending at least one portion of a gas from the mixing column to passages for warming the reboiler.
A process for the separation of air by cryogenic distillation for producing oxygen with a double column comprising:
- a medium-pressure column;
- and
- a low-pressure column which includes a reboiler for vaporizing liquid in the bottom of the low-pressure column,
- comprising the steps of:
- sending cooled and compressed air to the medium-pressure column;
- sending an oxygen-enriched liquid and a nitrogen-enriched liquid from the medium-pressure column to the low-pressure column;
- sending gas to the bottom of the mixing column;
- sending a second oxygen-enriched liquid from the low-pressure column to the top of the mixing column, the second liquid being less volatile than the gas feeding the bottom of the mixing column;
- withdrawing an oxygen-rich fluid from the low-pressure column;
- sending at least one portion of a gas from the mixing column to passages for warming the reboiler.
Process for the separation of air by cryogenic distillation for producing oxygen and optionally argon with a double column comprising:
- a medium-pressure column;
- a low-pressure column which includes a reboiler for vaporizing liquid in the bottom of the low-pressure column;
- and
- an argon column comprising a condenser and a mixing column,
- comprising the steps of:
- sending cooled and compressed air to the medium-pressure column,
- sending a first oxygen-enriched liquid from the medium-pressure column to the condenser;
- withdrawing an argon-enriched gas from a first level of the low-pressure column and sending the argon-enriched gas to the argon column;
- sending an oxygen enriched liquid and a nitrogen-enriched liquid from the medium-pressure column to the low-pressure column;
- at least partially vaporizing oxygen-enriched liquid in the condenser and sending at least one portion of the vapor and/or air to the bottom of the mixing column;
- sending a second oxygen-enriched liquid from the low-pressure column to the top of the mixing column, the second liquid being less volatile than the gas feeding the bottom of the mixing column;
- withdrawing an argon-enriched liquid from the top of the argon column;
- withdrawing an argon-enriched liquid from the top of the argon column;
- withdrawing an oxygen-rich fluid from the low-pressure column;
- and
- sending at least one portion of a gas from the mixing column to passages for warming the reboiler.
Dependencies are inferred from the claim text.