Crystal growth and annealing method and apparatus
AssigneesSandia Corporation, Corning Incorporated
InventorsSteven E. Gianoulakis, Robert Sparrow
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AssigneesSandia Corporation, Corning Incorporated
InventorsSteven E. Gianoulakis, Robert Sparrow
Estimating the term…
A method and apparatus for producing crystals that minimizes birefringence even at large crystal sizes, and is suitable for production of CaF2 crystals. The method of the present invention comprises annealing a crystal by maintaining a minimal temperature gradient in the crystal while slowly reducing the bulk temperature of the crystal. An apparatus according to the present invention includes a thermal control system added to a crystal growth and annealing apparatus, wherein the thermal control system allows a temperature gradient during crystal growth but minimizes the temperature gradient during crystal annealing. An embodiment of the present invention comprises a secondary heater incorporated into a conventional crystal growth and annealing apparatus. The secondary heater supplies heat to minimize the temperature gradients in the crystal during the annealing process. The secondary heater can mount near the bottom of the crucible to effectively maintain appropriate temperature gradients.
A crystal growth and annealing apparatus suitable for production of a fluoride crystal with minimized residual stress and birefringence, comprising:
A crystal annealing apparatus suitable for production of a fluoride crystal with minimized residual stress and birefringence, comprising
A crystal growth and annealing apparatus, comprising:
Dependencies are inferred from the claim text.