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US 6,306,194 B1Granted
Controlled release urea-formaldehyde liquid fertilizer resins with high nitrogen levels
AssigneeGeorgia-Pacific Resins, Inc.
InventorsStacey L. Wertz, Lisa M. Arthur, George E. Mirous, Kurt D. Gabrielson
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Abstract
A controlled release liquid urea formaldehyde fertilizer which has a nitrogen level at least 31% and its method of manufacture.
Claims11
A method of producing a urea-formaldehyde resin comprising:
- 1) combining formaldehyde, urea, and ammonia in a basic solution at a formaldehyde/urea/ammonia ratio of about 5.4-3.6/1/0.45-0.65;
- 2) heating the solution to about 85 to about 95° C., and holding to ensure triazone formation;
- 3) cooling the solution to less than about 50° C., and adjusting the pH to about 9.5 to about 10.5;
- 4) adding sufficient urea and ammonia to the solution to change the ratios to about 1.1-0.6/1/0.11-0.08;
- 5) reheating the solution to about 80° C. to about reflux, at a pH of between about 9 and about 11, for about 1 to about 2.5 hours;
- and
- 6) post charging urea to bring the mole ratio to about 0.9-0.6/1/0.1-0.08;
- wherein the nitrogen content of the resin is at least about 31% based on 100% resin solids.
5 more elements
Dependencies are inferred from the claim text.